The novel concept of NORD (NO relaxation delay) NMR spectroscopy is introduced. The idea is to design concatenated experiments in a way that the magnetization used in the first relaxes toward equilibrium during the second and vice versa, thus saving instrument time. Applications include complete well-resolved H- H and H- C one-bond and long-range correlation maps of an 80 mM solution of a trisaccharide recorded in less than two minutes and hydrocortisone with extensive spectral overlap.
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| http://www.ncbi.nlm.nih.gov/pmc/articles/PMC8252012 | PMC |
| http://dx.doi.org/10.1002/anie.202102487 | DOI Listing |
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