Background/purpose: Increasing the bond strength between the orthodontic brackets and all-ceramic materials is one of the challenges facing orthodontists. The purpose of this study is to assess the shear bond strength (SBS) of metal brackets to two types of all ceramic materials using various surface mechanical and chemical conditioning methods.
Materials And Methods: Sixty ceramic blocks were prepared using two types of all ceramic materials (IPS e.max and VITA Suprinity® PC) and treated with 3 surface treatments; surface etching with 9.6% hydrofluoric acid (HFA) for 2 mins; surface roughening with Sof-Lex finishing discs; and surface roughening with Sof-Lex finishing discs and etching with HFA. Metal brackets were attached to the surface of the ceramic blocks using light cure orthodontic adhesive. Samples were subjected to 2000 thermo-cycles (5-50 °C) and the SBS was assessed using Instron machine. The adhesive remnant index (ARI) was evaluated under light microscope. Descriptive and group comparison were calculated using Two-way ANOVA, Post-hoc Tukey's and Chi-square tests and significance level set at (P < 0.05).Results: surface roughening of both ceramic materials with Sof-Lex discs and HFA resulted in a significant increase in SBS compared to other experimental groups (P < 0.05). However, VITA Suprinity ceramic prepared with Sof-Lex discs only showed the lowest SBS. The distribution of the ARI scores was significantly different between the groups (P < 0.05).
Conclusion: Surface preparation of all ceramic materials with Sof-Lex discs and hydrofluoric acid combination produces the highest SBS to metallic orthodontic brackets.
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http://www.ncbi.nlm.nih.gov/pmc/articles/PMC7770247 | PMC |
http://dx.doi.org/10.1016/j.jds.2020.02.003 | DOI Listing |
ACS Nano
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Functional Materials Research Laboratory, School of Materials Science and Engineering, Tongji University, Shanghai 201804, P. R. China.
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Department of Material Science and Engineering, NTNU Norwegian University of Science and Technology, Trondheim 7491, Norway.
The chemical flexibility of the tetragonal tungsten bronze (TTB) structure offers a large potential for compositional engineering. Cation size and vacancy concentration are known to affect its structure, cation disorder, and functional properties. However, the compositional complexity also makes the TTB structure challenging to understand.
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College of Materials Science and Engineering, Hunan Joint International Laboratory of Advanced Materials and Technology of Clean Energy, Hunan Province Key Laboratory for Advanced Carbon Materials and Applied Technology, Hunan University, Changsha 410082, China.
Solid-state metallic potassium batteries (SSMPBs) afresh have attracted incremental attention because of their potential to supplement solid-state metallic lithium batteries. However, SSMPBs suffer poor electrochemical performances due to the low ionic conductivity of solid electrolytes and huge electrode/electrolyte interfacial resistance. Herein, high-rate SSMPBs are achieved by in situ ring-opening polymerization of 1,3-dioxolane with succinonitrile as a plasticizer and Al(OTf) as the catalyst, where the succinonitrile enables short-chain polyether electrolytes.
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National Innovation Center for Industry-Education Integration of Energy Storage Technology, College of Materials Science and Engineering, Chongqing University, Chongqing 400044, China.
Rechargeable magnesium ion batteries (RMBs) have drawn extensive attention due to their high theoretical volumetric capacity and low safety hazards. However, divalent Mg ions suffer sluggish mobility in cathodes owing to the high charge density and slow insertion/extraction kinetics. Herein, it is shown that an ultrafast nonequilibrium high-temperature shock (HTS) method with a high heating/quenching rate can instantly introduce oxygen vacancies into the olivine-structured MgFeSiO cathode (MgFeSiO-HTS) in seconds.
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Materials Science Innovation and Modelling (MaSIM) Research Focus Area, Faculty of Natural and Agricultural Sciences, North-West University, Mafikeng Campus, Private Bag X2046, Mmabatho, 2735, South Africa.
Hybrid wastewater treatment systems offer viable solutions to enhance the removal of complicated contaminants from aqueous system. This innovation has opened new avenues for advanced wastewater treatment processes. Herein, a novel TiO-ZnO functionalized coal fly ash-based ceramic membrane was fabricated by utilizing a combined pressing and sintering method.
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