Scanning Transmission Electron Microscopy Diffraction Contrast Imaging (STEM-DCI) has been gaining popularity for the identification and analysis of dislocations in crystalline materials due to its ability to supress undesirable image features that are often present in conventional TEM images. However, there does not yet exist a robust body of work demonstrating expected contrast in these imaging conditions. A novel approach for the simulation of STEM-DCI images was developed using a modified form of the scattering matrix formalism. This algorithm was used to simulate a variety of dislocation configurations generated using three-dimensional discrete dislocation dynamics.

Download full-text PDF

Source
http://dx.doi.org/10.1016/j.ultramic.2020.113124DOI Listing

Publication Analysis

Top Keywords

scanning transmission
8
transmission electron
8
electron microscopy
8
discrete dislocation
8
dislocation dynamics
8
contrast imaging
8
microscopy image
4
image simulations
4
simulations complex
4
dislocation
4

Similar Publications

This study explores the development and characterization of lyophilized chondroitin sulfate (CHON)-loaded solid lipid nanoparticles (SLN) as an innovative platform for advanced drug delivery. Solid lipid nanoparticles are increasingly recognized for their biocompatibility, their ability to encapsulate diverse compounds, their capacity to enhance drug stability, their bioavailability, and their therapeutic efficacy. CHON, a naturally occurring glycosaminoglycan with anti-inflammatory and regenerative properties, was integrated into SLN formulations using the hot microemulsion technique.

View Article and Find Full Text PDF

The study aimed to develop a superhydrophobic coating on the aluminium alloy 2024-T3 surface. The desired surface roughness and low surface energy were achieved with SiO nanoparticles, synthesised via the Stöber method and modified with alkyl silane (AS) or perfluoroalkyl silane (FAS). To enhance particle adhesion to the alloy substrate, nanoparticles were incorporated into a hybrid sol-gel coating composed of tetraethyl orthosilicate, methyl methacrylate, and 3-methacryloxypropyl trimethoxysilane.

View Article and Find Full Text PDF

This study explores the potential for the synthesis of peptide nanosystems comprising spinorphin molecules (with rhodamine moiety: Rh-S, Rh-S5, and Rh-S6) conjugated with nanoparticles (AuNPs), specifically peptide Rh-S@AuNPs, peptide Rh-S5@AuNPs, and peptide Rh-S6@AuNPs, alongside a comparative analysis of the biological activities of free and conjugated peptides. The examination of the microstructural characteristics of the obtained peptide systems and their physicochemical properties constitutes a key focus of this study. Zeta (ζ) potential, Fourier transformation infrared (FTIR) spectroscopy, circular dichroism (CD), scanning electron microscopy (SEM-EDS), transmission electron microscopy (TEM), and UV-Vis spectrophotometry were employed to elucidate the structure-activity correlations of the peptide@nano AuNP systems.

View Article and Find Full Text PDF

Fischer-Tropsch synthesis (FTS) in a 3D-printed stainless steel (SS) microchannel microreactor was investigated using Fe@SiO catalysts. The catalysts were prepared by two different techniques: one pot (OP) and autoclave (AC). The mesoporous structure of the two catalysts, Fe@SiO (OP) and Fe@SiO (AC), ensured a large contact area between the reactants and the catalyst.

View Article and Find Full Text PDF

Sonochemical Functionalization of SiO Nanoparticles with Citric Acid and Monoethanolamine and Its Remarkable Effect on Antibacterial Activity.

Materials (Basel)

January 2025

Centro de Investigación y de Estudios Avanzados del IPN-Unidad Mérida, Departamento de Física Aplicada, Mérida 97310, Yucatán, Mexico.

Nanoparticles (NPs) are excellent antibacterial agents due to their ability to interact with microorganisms at the cellular level. However, their antimicrobial capacity can be limited by their tendency to agglomerate. Functionalizing NPs with suitable ligands improves their stability and dispersion in different media and enhances their antibacterial activity.

View Article and Find Full Text PDF

Want AI Summaries of new PubMed Abstracts delivered to your In-box?

Enter search terms and have AI summaries delivered each week - change queries or unsubscribe any time!