Angular super-resolution retrieval in small-angle X-ray scattering.

Sci Rep

The Raymond and Beverly Sackler School of Physics and Astronomy, Tel Aviv University, 69978, Tel Aviv, Israel.

Published: September 2020

Small-angle X-ray scattering (SAXS) techniques enable convenient nanoscopic characterization for various systems and conditions. Unlike synchrotron-based setups, lab-based SAXS systems intrinsically suffer from lower X-ray flux and limited angular resolution. Here, we develop a two-step retrieval methodology to enhance the angular resolution for given experimental conditions. Using minute hardware additions, we show that translating the X-ray detector in subpixel steps and modifying the incoming beam shape results in a set of 2D scattering images, which is sufficient for super-resolution SAXS retrieval. The technique is verified experimentally to show superior resolution. Such advantages have a direct impact on the ability to resolve finer nanoscopic structures and can be implemented in most existing SAXS apparatuses both using synchrotron- and laboratory-based sources.

Download full-text PDF

Source
http://www.ncbi.nlm.nih.gov/pmc/articles/PMC7525553PMC
http://dx.doi.org/10.1038/s41598-020-73030-2DOI Listing

Publication Analysis

Top Keywords

small-angle x-ray
8
x-ray scattering
8
angular resolution
8
angular super-resolution
4
super-resolution retrieval
4
retrieval small-angle
4
x-ray
4
scattering small-angle
4
saxs
4
scattering saxs
4

Similar Publications

The rapid advancement of covalent organic frameworks (COFs) in recent years has firmly established them as a new class of molecularly precise and highly tuneable porous materials. However, compared to other porous materials, such as zeolites and metal-organic frameworks, the successful integration of hierarchical porosity into COFs remains largely unexplored. The challenge lies in identifying appropriate synthetic methods to introduce secondary pores without compromising the intrinsic structural porosity of COFs.

View Article and Find Full Text PDF

The vertebrate visual cycle hinges on enzymatically converting all--retinol (at-ROL) into 11--retinal (11c-RAL), the chromophore that binds to opsins in photoreceptors, forming light-responsive pigments. When struck by a photon, these pigments activate the phototransduction pathway and initiate the process of vision. The enzymatic isomerization of at-ROL, crucial for restoring the visual pigments and preparing them to receive new light stimuli, relies on various enzymes found in both the photoreceptors and retinal pigment epithelium cells.

View Article and Find Full Text PDF

Inter-Domain interactions Slow BoNT/A's onset of action.

J Struct Biol

January 2025

Department of Biochemical Engineering, University College London, London, United Kingdom.

Despite sharing ∼ 43 % sequence identity and structurally similar individual domains, botulinum neurotoxin (BoNT) serotypes A and E have differences in their properties and domain positioning. BoNT/E has a faster onset of action than BoNT/A. This difference is proposed to be due to conformational differences between BoNT/E and the other BoNT serotypes.

View Article and Find Full Text PDF

Deep eutectic solvents are highly tailorable non-aqueous solvents with potential applications ranging from energy catalysis to cryopreservation. Self-assembled lipid structures are already used in a variety of industries including cosmetics, drug delivery and as microreactors. However, most research into lipid self-assembly has been limited to aqueous solvents.

View Article and Find Full Text PDF

Mesoporous silica exhibits a diverse range of applications owing to its pore structure and inter-pore correlation. Consequently, quantitative characterization of its mesoscopic structure is extremely crucial to reciprocate its potential applications. In this work, we utilized the chemical and aerosol routes to successfully synthesize granular, porous silica with an average pore size in the range of ∼5-10 nm and different degrees of structural correlation among its pores.

View Article and Find Full Text PDF

Want AI Summaries of new PubMed Abstracts delivered to your In-box?

Enter search terms and have AI summaries delivered each week - change queries or unsubscribe any time!