Aluminum Melt Filtration with Carbon Bonded Alumina Filters.

Materials (Basel)

Institute of Ceramic, Glass and Construction Materials, Technische Universität Bergakademie Freiberg, Agricolastraße 17, 09599 Freiberg, Germany.

Published: September 2020

The wetting behavior was measured for AlO-C in contact with AlSi7Mg with a conventional sessile drop test (vacuum, 950 °C and 180 min) and a sessile drop test with a capillary purification unit (vacuum, 730 °C and 30 min). The conventional test yielded contact angles of around 92°, whereas the sessile drop measurement with capillary purification showed a strongly non-wetting behavior with a determined apparent contact angle of the rolling drop of 157°. Filtration tests, which were repeated twice, showed that the AlO-C filter possessed a better filtration behavior than the AlO reference filter. For both filtration trials, the PoDFA (porous disc filtration analysis) index of the AlO-C filter sample was equal to half of the PoDFA index of the AlO reference filter sample, indicating a significantly improved filtration performance when using AlO-C filter. Notable is the observation of a newly formed layer between the aluminum and the AlO-C coating. The layer possessed a thickness between 10 µm up to 50 µm and consisted of Al, C, and O, however, with different ratios than the original AlO-C coating. Thermodynamic calculations based on parameters of the wetting and filtration trials underline the possible formation of an AlOC-layer.

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http://www.ncbi.nlm.nih.gov/pmc/articles/PMC7559570PMC
http://dx.doi.org/10.3390/ma13183962DOI Listing

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