The effects of heat treatment on the microstructure evolution was studied in regards to austenite nucleation and grain growth. It was found that the austenite nucleation and matrix recrystallization kinetics of samples annealed at 675 °C for different times were revealed, implying a strong interaction between the ferrite matrix and austenite was revealed. The recrystallization of the matrix during annealing provided favorable conditions for austenite nucleation and growth, and the formation of austenite during this process reduced the matrix recrystallization kinetics, thus delaying the recrystallization process of the matrix around the austenite grains. The statistical results for the austenite grain size under different annealing temperatures indicated that the average grain size of the austenite slightly increases with increasing of the annealing temperature, but the austenite with the largest grain size grows faster at the same temperature. This difference is attributed to the strict Kurdjumov Sachs (KS) orientation relationship (OR) between the austenite grains and the matrix, because the growth of austenite with a strict KS OR with the matrix is often inhibited during annealing. In contrast, the austenite maintains a non-strict KS OR with the matrix and can grow preferentially with increasing annealing temperature and time.
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http://dx.doi.org/10.3390/ma13153366 | DOI Listing |
BMC Oral Health
January 2025
Department of Conservative Dentistry, College of Dentistry, Kyung Hee University, 26-6, Kyungheedae-ro, Dongdaemun-gu, Seoul, 02453, Republic of Korea.
Background: This study aims to compare design, phase transformation behavior, and torsional resistance of the ProGlider (PG) and ProTaper ultimate slider (PUS) and to compare the performance of two files in the glide-path preparation of a double-curved artificial canal.
Methods: Scanning electron microscopy, micro-computed tomography, and differential scanning calorimetry were used to characterize the samples. A torsional resistance test was performed to obtain ultimate strength and distortion angle.
Materials (Basel)
January 2025
Faculty of Metallurgical and Energy Engineering, Kunming University of Science and Technology, Kunming 650031, China.
Fracture toughness is an important index related to the service safety of marine risers, and weld is an essential component of the steel catenary risers. In this paper, microscopic structure characterization methods such as scanning electron microscopy (SEM) and electron back scatter diffraction (EBSD), as well as mechanical experiments like crack tip opening displacement (CTOD) and nanoindentation, were employed to conduct a detailed study on the influence of the microstructure characteristics of multi-wire submerged arc welded seams of steel catenary riser pipes on CTOD fracture toughness. The influence mechanisms of each microstructure characteristic on fracture toughness were clarified.
View Article and Find Full Text PDFMaterials (Basel)
January 2025
Faculty of Engineering, Kitami Institute of Technology, 165 Koen-cho, Kitami 090-8507, Hokkaido, Japan.
The addition of hydrogen to nitrogen facilitates the formation of nitride phases in the plasma nitriding processes of stainless steels, though it also induces the deterioration of their mechanical properties. This study presents a hydrogen-free plasma nitriding process for fabricating a nitrogen-expanded austenite phase (γ) on an AISI 316 stainless steel surface. The steel substrate was nitrided in N-Ar plasma with various gas compositions discharged by radio frequency (RF) and direct current (DC) modes.
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December 2024
School of Material Science and Engineering, Huazhong University of Science & Technology, Wuhan 430074, China.
W-Mo-V high-speed steel (HSS) is a high-alloy high-carbon steel with a high content of carbon, tungsten, chromium, molybdenum, and vanadium components. This type of high-speed steel has excellent red hardness, wear resistance, and corrosion resistance. In this study, the alloying element ratios were adjusted based on commercial HSS powders.
View Article and Find Full Text PDFMaterials (Basel)
December 2024
School of Materials Science and Engineering, Shanghai University, Shanghai 200444, China.
In this study, a novel Cu-bearing 304 stainless steel doped with 4.0 wt.% Cu (304-Cu SS) was developed, and the effects of nitrogen microalloying (304N-Cu SS) and heat treatment on mechanical, antibacterial, and corrosion properties were investigated.
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