AI Article Synopsis

  • Crystalline lattice structures significantly influence materials' functional properties such as elasticity and magnetism, making orientation determination tools highly valuable.
  • Surface acoustic wave (SAW) velocity measurements can effectively identify crystallographic orientations, particularly in cubic materials, but there's a need for improved methods in anisotropic crystals like hexagonal close packed titanium.
  • The study combines experimental and simulation data to analyze the effects of different parameters on orientation accuracy, demonstrating that precise control can lead to errors in orientation determination being minimized to less than 1°, nearing theoretical limits.

Article Abstract

Throughout our engineered environment, many materials exhibit a crystalline lattice structure. The orientation of such lattices is crucial in determining functional properties of these structures, including elasticity and magnetism. Hence, tools for determining orientation are highly sought after. Surface acoustic wave velocities in multiple directions can not only highlight the microstructure contrast, but also determine the crystallographic orientation by comparison to a pre-calculated velocity model. This approach has been widely used for the recovery of orientation in cubic materials, with accurate results. However, there is a demand to probe the microstructure in anisotropic crystals - such as hexagonal close packed titanium. Uniquely, hexagonal structure materials exhibit transverse isotropic linear elasticity. In this work, both experimental and simulation results are used to study the discrete effects of both experimental parameters and varying lattice anisotropy across the orientation space, on orientation determination accuracy. Results summarise the theoretical and practical limits of hexagonal orientation determination by linear SAW measurements. Experimental results from a polycrystalline titanium specimen, obtained by electron back scatter diffraction and spatially resolved acoustic spectroscopy show good agreement (errors of ϕ=5.14° and Φ=6.99°). Experimental errors are in accordance with those suggested by simulation, according to the experimental parameters. Further experimental results demonstrate dramatically improved orientation results (Φ error <1°). Demonstrating the possibility of achieving results near the theoretical limit by strict control of the experimental parameters.

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Source
http://dx.doi.org/10.1016/j.ultras.2020.106171DOI Listing

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