An efficient laboratory method to measure the combined effects of Knudsen diffusion and mechanical deformation on shale permeability.

In a shale gas reservoir, the rock matrix has a relatively large porosity and gas in place, but extremely low permeability. Thus, the rock matrix is a bottleneck for shale gas flow from the reservoir to hydraulic fractures and then to the production well. We speculate that the next big thing after hydraulic fracturing for unconventional resources development is to enhance the matrix permeability in an economically feasible way. Consequently, the efficient and accurate characterization of rock matrix permeability in the laboratory is a critical task. The current laboratory techniques for source rock permeability measurement follow a "point-by-point" approach. They need multiple test runs to obtain a permeability-pressure curve, because they can only measure one permeability data point for one test run, and are thus time consuming. The root cause of this "point-by-point" approach is that these laboratory techniques are based on linearized gas flow theory requiring only small pore pressure disturbances to the experiment system. Liu et al. (2019) and this work introduce a new methodology that is based on the nonlinear gas flow theory and allows for direct measurement of the permeability-pressure curve with a single test run. This makes the approach highly time efficient. The feasibility and validity of the methodology are demonstrated in this work based on laboratory measurement results and their consistency with theoretical expectations and other independent measurements. The observed permeability exhibits a complex relationship with pore pressure as a result of the combined effects of Knudsen diffusion and mechanical deformation. For a given confining pressure, the observed permeability initially decreases with pore pressure because of Knudsen diffusion and then increases with pore pressure owing to the mechanical deformation. A rock sample with a lower permeability corresponds to a stronger Knudsen diffusion effect and weaker mechanical diffusion effect. This complex behavior highlights the need to accurately and efficiently measure the combined effects that may have important impacts on shale gas production.