AI Article Synopsis

  • The paper investigates how to effectively select etching methods for revealing the microstructure of CMSX-4 nickel-based superalloy through metallographic techniques.
  • It outlines a variety of chemical and electrochemical etching methods and analyzes their impacts by taking microphotographs with optical and scanning electron microscopes after each process.
  • The study emphasizes the importance of choosing the appropriate etching methodology, showcasing how it affects the qualitative and quantitative analysis of the microstructure findings.

Article Abstract

The paper presents the findings of a research on the selection of methodology for revealing the microstructure in metallographic investigations on the example of the single-crystalline CMSX-4 nickel-based superalloy. A set of chemical and electrochemical methods of etching has been selected. The metallographic specimens from the analyzed material have been treated with the etchants. After every etching procedure, microphotographs of the microstructure were taken by means of an optical microscope and a scanning electron microscope. Both useful and disadvantageous effects of etching with the respective etchants have been displayed. The etchant application for a qualitative and quantitative analysis has been considered on the basis of the enclosed microphotographs. As a result, examples of a computer-aided detection of the phases and microstructural constituents present in the analyzed CMSX-4 alloy for the selected revealing methodologies have been demonstrated. The described investigations enable a better understanding of the essence of the selection of the microstructure revealing methodology and its influence on the obtained results.

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Source
http://www.ncbi.nlm.nih.gov/pmc/articles/PMC7014115PMC
http://dx.doi.org/10.3390/ma13020341DOI Listing

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