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Electrochemical Oxidative Oxydihalogenation of Alkynes for the Synthesis of α,α-Dihaloketones. | LitMetric
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Electrochemical Oxidative Oxydihalogenation of Alkynes for the Synthesis of α,α-Dihaloketones.

Xiangtai Meng Yu Zhang Jinyue Luo Fei Wang Xiaoji Cao Shenlin Huang

Org Lett

Jiangsu Provincial Key Lab for the Chemistry and Utilization of Agro-Forest Biomass, College of Chemical Engineering, Jiangsu Key Lab of Biomass-Based Green Fuels and Chemicals, Jiangsu Co-Innovation Center of Efficient Processing and Utilization of Forest Resources , Nanjing Forestry University, Nanjing 210037 , P. R. China.

Published: February 2020

An electrochemical oxydihalogenation of alkynes has been developed for the first time. Using this sustainable protocol, a variety of α,α-dihaloketones can be prepared with readily available CHCl, CHCl, ClCHCHCl, and CHBr as the halogen source under electrochemical conditions at room temperature.

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http://dx.doi.org/10.1021/acs.orglett.0c00052DOI Listing

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