Classical methods of material testing become extremely complicated or impossible at micro-/nanoscale. At the same time, depth-sensing indentation (DSI) can be applied without much change at various length scales. However, interpretation of the DSI data needs to be done carefully, as length-scale dependent effects, such as adhesion, should be taken into account. This review paper is focused on different DSI approaches and factors that can lead to erroneous results, if conventional DSI methods are used for micro-/nanomechanical testing, or testing soft materials. We also review our recent advances in the development of a method that intrinsically takes adhesion effects in DSI into account: the Borodich-Galanov (BG) method, and its extended variant (eBG). The BG/eBG methods can be considered a framework made of the experimental part (DSI by means of spherical indenters), and the data processing part (data fitting based on the mathematical model of the experiment), with such distinctive features as intrinsic model-based account of adhesion, the ability to simultaneously estimate elastic and adhesive properties of materials, and non-destructive nature.
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http://dx.doi.org/10.3390/nano10010015 | DOI Listing |
Am J Orthod Dentofacial Orthop
January 2025
Departments of Materials Science and Engineering and Bioengineering, University of Texas at Dallas, Richardson, Tex.
Introduction: This study aimed to identify the link between alloy microstructures and the nanomechanical properties of different orthodontic archwires containing nickel-titanium (NiTi) by sensing sliced areas. Previous studies have focused on analyzing and contrasting physical properties such as microhardness, elasticity modulus, and resistance; therefore, the trend is to consider microstructural characteristics in detail.
Methods: Thirty archwire samples from 3 different commercial brands, American Orthodontics (AO), 3M Unitek (3M), and Borgatta, were analyzed through scanning electron microscopy and energy-dispersive x-ray spectroscopy, transmission electron microscopy, atomic force microscopy, Berkovich nanoindentation, and microtensile microscopy to determine their chemical-crystallographic characteristics and nanomechanical and bending characteristics.
Sci Rep
September 2024
CAS Key Laboratory of Carbon Materials, Institute of Coal Chemistry, Chinese Academy of Sciences, Taiyuan, 030001, China.
Materials (Basel)
May 2024
SaMASZ Sp. z o.o., ul. Trawiasta 1, 16-060 Zabludow, Poland.
The paper presents an analysis of the low-cycle fatigue (LCF) properties of C45, X20Cr13, and 34CrNiMo6 steels subjected to various heat treatment processes. Strain-controlled LCF tests were carried out with a total cyclic strain amplitude equal to 0.5, 1 and 1.
View Article and Find Full Text PDFMaterials (Basel)
October 2023
Department of Materials Physics, Eötvös Loránd University, Pázmány Péter Sétány 1/A, 1117 Budapest, Hungary.
A supersaturated Al-4.8%Zn-1.2%Mg-0.
View Article and Find Full Text PDFJ Mech Behav Biomed Mater
November 2023
Department of Metallurgy and Structural Integrity, National Nanotechnology Laboratory Centro de Investigación en Materiales Avanzados S.C, Chihuahua, Chihuahua, Mexico. Electronic address:
This article focuses on a description of research performed to identify structural and mechanical properties differences between calculi in stones, such as gallstones, kidney stones, dental tartar, and saliva gland sialolite, were analyzed and compared with tap water stone, in order to set interrelations. In this study, biological hard pebble-like structures were analyzed and compared among them using Scanning Electron Microscopy (SEM), X-Ray diffraction (XRD), and Atomic Force Microscopy (AFM). In addition, Nanoindentation was used to obtain values as example in kidney stones the in; stiffness S = 27,827 ± 620 N/nm elastic modulus E = 27.
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