BiTe nanowires with diameters ranging from 25 to 270 nm, ultra-high aspect ratio, and uniform growth front were fabricated by electrodeposition, pulsing between zero current density during the time and constant potential during the time (pulsed-current-voltage method, p-IV). The use of zero current density during the time is to ensure no electrodeposition is carried out and the system is totally relaxed. By this procedure, stoichiometric nanowires oriented perpendicular to the is obtained for the different diameters of porous alumina templates. In addition, the samples show a uniform growth front with ultra-high aspect ratio single crystal nanowires. The high degree of crystallinity was verified by transmission electron backscatter diffraction. This characterization revealed that the nanowires present both large single crystalline areas and areas with alternating twin configurations.
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http://dx.doi.org/10.1080/14686996.2019.1671778 | DOI Listing |
J Phys Condens Matter
March 2021
Indian Institute of Science Education and Research Thiruvananthapuram, Kerala 695551, India.
The lattice heat transport properties of the thermoelectric (TE) material SnTe and the doped SnSbTe and SnBiTe are examined using Boltzmann transport theory supplemented with first-principle calculations. We illustrate the microscopic origin of the lattice thermal conductivity, κ of the materials by calculating the mode Grüneisen parameters, phase space volume for three-phonon processes, the anharmonic scattering rates (SR), and the phonon group velocities. SnTe is found to be a low κ material with a value of ∼3 W mK at room temperature in agreement with experiments.
View Article and Find Full Text PDFNanoscale Adv
January 2021
Novel Materials Group, Humboldt-Universität zu Berlin 10099 Berlin Germany
We demonstrate the full thermoelectric and structural characterization of individual bismuth-based (Bi-based) core/shell nanowires. The influence of strain on the temperature dependence of the electrical conductivity, the absolute Seebeck coefficient and the thermal conductivity of bismuth/titanium dioxide (Bi/TiO) nanowires with different diameters is investigated and compared to bismuth (Bi) and bismuth/tellurium (Bi/Te) nanowires and bismuth bulk. Scattering at surfaces, crystal defects and interfaces between the core and the shell reduces the electrical conductivity to less than 5% and the thermal conductivity to less than 25% to 50% of the bulk value at room temperature.
View Article and Find Full Text PDFJ Electromyogr Kinesiol
February 2021
Department of Oral Rehabilitation, University of Otago, Dunedin, New Zealand.
Objectives: The study investigated effects of electrode material, inter-electrode distance (IED), and conductive gel on electromyographic (EMG) activity recorded from the masseter muscle.
Materials And Methods: EMG was recorded unilaterally, as ten volunteers performed standardized oral tasks. Ag/AgCl and Ag coated with Au were the gel-based; Ag alloy coated with graphene, pure Ag coated with graphene and silver nanowire embedded electrodes were the gel-free materials tested.
ACS Omega
May 2019
Chemical and Chemical Technology Department, Bronx Community College, The City University of New York, Bronx, New York 10453, United States.
Nanomaterials (Basel)
May 2018
Instituto de Micro y Nanotecnología, IMN-CNM, CSIC (CEI UAM+CSIC) Isaac Newton, 8, E-28760 Madrid, Spain.
Self-standing Bi₂Te₃ networks of interconnected nanowires were fabricated in three-dimensional porous anodic alumina templates (3D⁻AAO) with a porous structure spreading in all three spatial dimensions. Pulsed electrodeposition parameters were optimized to grow highly oriented Bi₂Te₃ interconnected nanowires with stoichiometric composition inside those 3D⁻AAO templates. The nanowire networks were analyzed by X-ray diffraction (XRD), scanning electron microscopy (SEM), energy dispersive X-ray analysis (EDX), and Raman spectroscopy.
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