Improved calibration of area detectors using multiple placements.

J Synchrotron Radiat

Advanced Photon Source, Argonne National Laboratory, 9700 S. Cass Avenue, Lemont, IL 60439, USA.

Published: November 2019

Calibration of area detectors from powder diffraction standards is widely used at synchrotron beamlines. From a single diffraction image, it is not possible to determine both the sample-to-detector distance and the wavelength, but, with images taken from multiple positions along the beam direction and where the relative displacement is known, the sample-to-detector distance and wavelength can both be determined with good precision. An example calibration using the GSAS-II software package is presented.

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http://www.ncbi.nlm.nih.gov/pmc/articles/PMC6853381PMC
http://dx.doi.org/10.1107/S1600577519013328DOI Listing

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