H relaxometry measurements of petroleum core plugs are commonly performed on low field magnets (<0.5 Tesla) to reduce the influence of magnetic susceptibility mismatch on measurements of the spin-spin relaxation time, T. The Signal to Noise Ratio (SNR) of the MR signal, however, generally decreases with lower magnetic fields. Higher magnetic fields (>3 Tesla) are typically employed in small animal MRI studies to improve SNR and image resolution. For many rock core plug samples, susceptibility mismatch effects can be severe at these higher fields leading to decreased T and T*. In this work we seek an answer to the general question of what is the best field for MRI of rock core plugs, anticipating that it will be both sample and measurement method dependent. Free Induction Decay (FID) relaxation time measurements were undertaken to investigate the conditions under which the SNR in Centric Scan SPRITE (Single Point Ramped Imaging with T Enhancement) MRI measurements is maximized. The image SNR benefits from greater signal at higher fields, but is negatively impacted by the correspondingly shorter signal lifetimes. Depending on the noise regime of the sample, the maximum SNR may be predicted for Centric Scan SPRITE MRI with T* being B field dependent. In this work we describe a series of simple experimental considerations to determine the optimal B field for SPRITE MRI. Selection of the best field is aided by a new generation of superconducting magnets which allows the experimentalist to readily vary the field strength. Such magnets allow one to experimentally control sample magnetization for high sensitivity MRI measurements of core plug samples, while controlling the effect of susceptibility mismatch on the signal lifetimes.

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http://dx.doi.org/10.1016/j.jmr.2019.106575DOI Listing

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