We report, herein, a diamond-like oxysulfide framework, 3D-T4-SnOS, based on the largest supertetrahedral cluster of Sn ions, i.e. [SnOS]. The framework remains intact in aqueous solution over a pH range between 1 and 14, and has a narrower optical bandgap, red-shifted fluorescence emission, and an enhanced photoelectric response compared to that of the smaller version, 2D-T3-SnOS, which has a building unit of supertetrahedral [SnOS].
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