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http://dx.doi.org/10.5005/jp-journals-10071-23172 | DOI Listing |
J Org Chem
January 2025
College of Chemistry and Environmental Science, Qujing Normal University, Qujing, Yunnan 655011, China.
A novel metal- and azide-free methodology for the synthesis of trifluoromethylated 1,2,3-triazoles from arylamines with a new 3-bromo-1,1,1-trifluoropropan-2-one derived tosylhydrazone has been developed under mild reaction conditions. The new α-bromo-trifluoromethylated tosylhydrazone reagent was operationally safe and bench-stable from low-cost and readily commercially available starting materials in the iodine-promoted aerobic oxidative cycloaddition reaction with arylamines, affording a variety of trifluoromethylated 1,2,3-triazoles in good to excellent yields.
View Article and Find Full Text PDFNeurogastroenterol Motil
January 2025
Department of Pediatrics, Medical College of Wisconsin, Milwaukee, WI, USA.
Investigations into mechanisms of cyclic(al) vomiting syndrome (CVS) began at the bedside more than a century ago. The modern era started with the formation of the Cyclic Vomiting Syndrome Association in 1993 that helped initiate robust efforts in education, advocacy, family physician conferences, scientific symposia, dedicated clinical programs, therapeutic guidelines, and research. Even today, bedside clues continue to emerge with the recent description of cannabinoid hyperemesis syndrome (CHS) and subsequent evidence of a perturbed endocannabinoid system.
View Article and Find Full Text PDFJ Strength Cond Res
January 2025
School of Behavioural and Health Sciences, Australian Catholic University, Brisbane, Australia.
Cowley, N, Nicholson, V, Timmins, R, Munteanu, G, Wood, T, García-Ramos, A, Owen, C, and Weakley, J. The effects of percentage-based, rating of perceived exertion, repetitions in reserve, and velocity-based training on performance and fatigue responses. J Strength Cond Res XX(X): 000-000, 2024-This study assessed the effects of percentage-based training (%1RM), rating of perceived exertion (RPE), repetitions in reserve (RIR), and velocity-based training (VBT) on (a) acute kinematic outputs, perceptions of effort, and changes in neuromuscular function during resistance training; and (b) neuromuscular fatigue and perceptions of soreness 24 hours after exercise.
View Article and Find Full Text PDFFront Nutr
November 2024
Movement, Sport, Health and Sciences Laboratory (M2S), UFR APS, University of Rennes 2-ENS Cachan, Rennes, France.
J Bodyw Mov Ther
October 2024
School of Physical Education and Sports, Federal University of Rio de Janeiro, Rio de Janeiro, Brazil; LADTEF - Performance, Training, and Physical Exercise Laboratory, Federal University of Rio de Janeiro, Rio de Janeiro, Brazil.
Introduction: A warm-up is recommended prior to performing a resistance training workout. Understanding the dose-response effect of warm-up load intensities can contribute to subsequent workout performance. The aim of this study was to compare different warm-up load intensities on subsequent resistance training volume in a workout.
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