Expanded polystyrene (EPS) foam is widely used in building and construction applications for thermal and acoustic insulation. This material is nearly transparent for X-rays, making it difficult to characterize its pore structure in 3D with X-ray tomography. Because of this difficulty, the pore network is often not investigated and is, thus, poorly known. Since this network controls different physical properties, such as the sound absorption, it is crucial to understand its overall structure. In this manuscript, we show how to reveal the pore network of EPS foams through the combination of high resolution X-ray tomography (micro-CT) and saturation techniques. The foams were saturated with CsCl-brine, which acts as a contrasting agent in X-ray micro-CT imaging. This allowed us to separate the beads, making up the foam, from the pore network. Based on the 3D micro-CT results, we were able to assess a representative elementary volume for the polystyrene, which allows for calculating the acoustical parameters from the Johnson-Champoux-Allard (JCA) model, the pore and bead size distribution. The 3D data was also used as input to simulate sound absorption curves. The parametric study showed that an increase in the bead size influenced the sound absorption of the material. We showed that, by doubling the diameter of beads, the absorption coefficient was doubled in certain ranges of frequency.

Download full-text PDF

Source
http://www.ncbi.nlm.nih.gov/pmc/articles/PMC6630325PMC
http://dx.doi.org/10.3390/ma12121944DOI Listing

Publication Analysis

Top Keywords

pore network
12
sound absorption
12
expanded polystyrene
8
polystyrene eps
8
eps foam
8
x-ray tomography
8
bead size
8
pore
5
x-ray
4
x-ray computed
4

Similar Publications

Mesoporous silica exhibits a diverse range of applications owing to its pore structure and inter-pore correlation. Consequently, quantitative characterization of its mesoscopic structure is extremely crucial to reciprocate its potential applications. In this work, we utilized the chemical and aerosol routes to successfully synthesize granular, porous silica with an average pore size in the range of ∼5-10 nm and different degrees of structural correlation among its pores.

View Article and Find Full Text PDF

Guest transport through discrete voids (closed pores) in crystalline solids is poorly understood. Herein, we report the gas sorption properties of a nonporous coordination network, [Co(bib)2Cl2]n·2MeOH (sql-bib-Co-Cl-α), featuring square lattice (sql) topology and the bent linker 1,3-bis(1H-imidazol-1-yl)benzene (bib). The as-synthesized sql-bib-Co-Cl-α has 11.

View Article and Find Full Text PDF

Synthesis of pillar-layered metal-organic frameworks with variable backbones through sequence control.

Nat Chem

January 2025

Engineering Research Center of Photoenergy Utilization for Pollution Control and Carbon Reduction, Ministry of Education, State Key Laboratory of Green Pesticide, College of Chemistry, Central China Normal University, Wuhan, China.

The properties and functions of metal-organic frameworks (MOFs) can be tailored by tuning their structure, including their shape, porosity and topology. However, the design and synthesis of complex structures in a predictable manner remains challenging. Here we report the preparation of a series of isomeric pillar-layered MOFs, and we show that their three-dimensional topology can be controlled by altering the layer stacking.

View Article and Find Full Text PDF

Proton exchange membrane fuel cell (PEMFC) is considered the next promising generation of power devices for vehicles. The microporous layer (MPL) improves the performance through effective water management. In this study, local hydrophilic networks of nano- and macropores are formed in different MPLs.

View Article and Find Full Text PDF

Exploring the multifaceted roles of metal-organic frameworks in ecosystem regulation.

J Mater Chem B

January 2025

State Key Laboratory of Oral Diseases, National Clinical Research Center for Oral Diseases, West China Hospital of Stomatology, Sichuan University, Chengdu 610041, China.

Achieving microecological balance is a complex environmental challenge. This is because the equilibrium of microecological systems necessitates both the eradication of harmful microorganisms and preservation of the beneficial ones. Conventional materials predominantly target the elimination of pathogenic microorganisms and often neglect the protection of advantageous microbial species.

View Article and Find Full Text PDF

Want AI Summaries of new PubMed Abstracts delivered to your In-box?

Enter search terms and have AI summaries delivered each week - change queries or unsubscribe any time!