AI Article Synopsis

  • The Diamond Light Source (DLS) beamline I15-1 utilizes high-energy X-rays (40-80 keV) to analyze atomic pair distribution functions (PDF).
  • A specially designed, 1-meter-long multilayer-coated bimorph mirror focuses these X-rays into a precise spot size, optimizing their use in experiments.
  • The mirror successfully achieved focal spots with a vertical width of less than 15 µm and demonstrated effective adjustments for varying focal positions, marking a significant advancement in synchrotron beamline technology.

Article Abstract

The Diamond Light Source (DLS) beamline I15-1 measures atomic pair distribution functions (PDF) using scattering of 40-80 keV X-rays. A unique focusing element was needed to condense these X-rays from an initial large cross section (11.0 mm H × 4.2 mm V) into a required spot size of FWHM ≈680 μm (H) × 20 μm (V) at a variable position between the sample and the detector. The large numerical aperture is achieved by coating a silicon substrate over 1 m long with three multilayer stripes of Bragg angle 4.2 mrad. One stripe selects X-rays of each energy 40.0, 65.4, and 76.6 keV. Sixteen piezoelectric bimorph actuators attached to the sides of the mirror substrate adjusted the reflecting surface's shape. Focal spots of vertical width < 15 µm were obtained at three positions over a 0.92 m range, with fast, easy switching from one focal position to another. Minimized root mean square slope errors were close to 0.5 µrad after subtraction of a uniform curvature. Reflectivity curves taken along each stripe showed consistent high peaks with generally small angular variation of peak positions. This is the first application of a 1 m long multilayer-coated bimorph mirror at a synchrotron beamline. Data collected with its help on a slice of a lithium ion battery's cathode are presented.

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Source
http://dx.doi.org/10.1364/OE.27.016121DOI Listing

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