Many studies have been conducted on organic and inorganic synthesis by microwave heating owing to its special heating mechanism, leading to improved reaction rate, higher purity and yields. We specifically demonstrated microwave heating in the fabrication of nanoparticles and polyester. By fine-tuning the microwave and experimental parameters, the materials prepared have shown excellent physical and bio-properties, e. g. narrow particle size distribution, controlled morphology, varied molecular structure and so forth. We further highlight the recent procedure of using fluidic reactors on preparing both metals and metal oxides nanoparticles. The experimental design strategies and fundamentals of the microwave interaction with chemicals are presented. Furthermore, the key factors and issues facing in this area are also discussed.
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http://dx.doi.org/10.1002/tcr.201800121 | DOI Listing |
Nanotechnology
January 2025
Universiti Teknologi PETRONAS, Centre of Innovative Nanostructures and Nanodevices (COINN), Universiti Teknologi PETRONAS, 32610 Seri Iskandar, Perak Darul Ridzuan, MALAYSIA, Seri Iskandar, Perak, 32610, MALAYSIA.
Most previously reported susceptors for microwave welding are in powder form. In this study, a thin-film susceptor was employed due to its uniform heating rate and ease of handling. Silicon carbide nanowhisker (SiCNW) were incorporated into a poly(methyl methacrylate) (PMMA) matrix to create a nanocomposite thin film, which served as the susceptor.
View Article and Find Full Text PDFACS Appl Mater Interfaces
January 2025
School of Materials Science and Engineering, Harbin Institute of Technology, Harbin 150001, China.
Presently, researchers are placing emphasis on microwave absorption coating design while neglecting the research on materials that integrate both microwave absorption performance and mechanical properties. Here, robust FeSiAl/PEEK composites were prepared by a series process, including post ball-milling annealing, sol-gel method, and hot pressing. A detailed analysis of the electromagnetic (EM) parameters reveals the significant effects of morphology, filling ratio, and microstructure of FeSiAl on EM losses under a wide-temperature range.
View Article and Find Full Text PDFSmall
January 2025
School of Mechanical Engineering, Korea University, 145 Anam-Ro, Seongbuk-Gu, Seoul, 02841, Republic of Korea.
Passive temperature controls like passive daytime radiative cooling (PDRC)-heating (PDRH), and thermal insulation are essential to meet the growing demand for energy-efficient thermal solutions. When combined with advanced functions like electromagnetic interference shielding, these technologies can significantly enhance scalability. However, existing approaches using single thin films or uniform porous materials face inherent limitations in optimizing versatile functions, while lightweight, insulating aerogels can extend their multifunctionality by manipulating pores and fillers.
View Article and Find Full Text PDFRev Sci Instrum
January 2025
College of Public Health, Sichuan University, Chengdu 610041, China.
In this paper, a microwave thermal imaging system (MTIS) has been presented for debonding detection of radar absorbing materials (RAMs). First, an overview of the mechanism underlying microwave heating and the fundamental principle of defect detection within RAMs is presented. Then, a multifunctional MTIS capable of performing both microwave lock-in thermography (MLIT) and long-pulse microwave thermography (LPMT) has been introduced, specifically tailored for the in situ inspection of RAMs.
View Article and Find Full Text PDFSci Rep
January 2025
Institute of Agrophysics, Polish Academy of Sciences, Doświadczalna 4, Lublin, 20-290, Poland.
The main aim of the study was to develop new fruit waste-derived activated carbons of high adsorption performance towards metals, metalloids, and polymers by the use of carbon dioxide (CO)-consuming, microwave-assisted activation. The authors compared morphology, surface chemistry, textural parameters, and elemental composition of precursors (chokeberry seeds, black currant seeds, orange peels), as well as biochars (BCs) and activated carbons (ACs) obtained from them. The adsorption mechanisms of metals (copper, cadmium), metalloids (arsenic, selenium), and macromolecular compounds (bacterial exopolysaccharide, ionic polyacrylamides) on the surface of selected materials were investigated in one- and two-component systems.
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