We have designed and built a scanning tunneling microscope (STM) setup for operation at millikelvin temperatures in an ultrahigh vacuum. A compact cryostat with an integrated dilution refrigerator has been built that allows measurements at a base temperature of 25 mK in the magnetic field up to 7.5 T with low mechanical and electronic noise. The cryostat is not larger than conventional helium bath cryostats (23 and 13 l of nitrogen and helium, respectively) so that the setup does not require a large experimental hall and fits easily into a standard lab space. Mechanical vibrations with running dilution circulation were kept below 1 pm/ by mechanically decoupling the STM from the cryostat and the pumping system. All electronic input lines were low-pass filtered, reducing the electronic temperature to below 100 mK, as deduced from the quasiparticle peaks of superconducting aluminum. The microscope is optically accessible in the parked position, making sample and tip exchange fast and user-friendly. For measurement, the STM is lowered 60 mm down so that the sample ends in the middle of a wet superconducting magnetic coil.
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http://dx.doi.org/10.1063/1.5043636 | DOI Listing |
Subcell Biochem
December 2024
Department of Physics of the Condensed Matter, C03 and IFIMAC (Instituto de Física de la Materia Condensada). Universidad Autónoma de Madrid, Madrid, Spain.
Atomic force microscopy (AFM) makes it possible to obtain images at nanometric resolution, and to accomplish the manipulation and physical characterization of specimens, including the determination of their mechanical and electrostatic properties. AFM has an ample range of applications, from materials science to biology. The specimen, supported on a solid surface, can be imaged and manipulated while working in air, ultra-high vacuum or, most importantly for virus studies, in liquid.
View Article and Find Full Text PDFNanotechnology
December 2024
IEMN, avenue Poincaré, Villeneuve-d'Ascq, Hauts-de-France, 59652, FRANCE.
We report here the reversibility and bistability of the switching behavior in an azobenzene derivative induced by the bias applied by a Scanning-Tunneling Microscopy (STM) tip, at low temperature and in ultra-high vacuum environment. This cis-to-trans and trans-to-cis switching were observed during STM imaging in either polarity at +2V or -2V, on a sub-second time scale. This results in a blinking effect visible on STM images, corresponding to the reversible switching of the azobenzene molecule under the applied STM bias through an electric field induced process.
View Article and Find Full Text PDFRev Sci Instrum
December 2024
2nd Institute of Physics B and JARA-FIT, RWTH Aachen University, 52074 Aachen, Germany.
Low-temperature scanning tunneling spectroscopy is a key method to probe electronic and magnetic properties down to the atomic scale, but suffers from extreme vibrational sensitivity. This makes it challenging to employ closed-cycle cooling with its required pulse-type vibrational excitations, albeit this is mandatory to avoid helium losses for counteracting the continuously raising helium prices. Here, we describe a compact ultra-high vacuum scanning tunneling microscope (STM) system with an integrated primary pulse tube cooler (PTC) for closed-cycle operation.
View Article and Find Full Text PDFHeliyon
December 2024
Korea Railroad Research Institute, 176 Cheoldobangmulgwan-ro, Uiwang-si, Gyeonggi-do 16105, Republic of Korea.
This study evaluates the air permeability of epoxy-coated normal concrete and ultra-high performance concrete (UHPC) for use in Hyperloop tube structures, where maintaining ultra-low air permeability is crucial to preserving the vacuum environment. While UHPC is recognized for its exceptionally low permeability due to its dense microstructure, this research explores epoxy-coated conventional concrete as a cost-effective alternative. Using a vacuum-based permeability test simulating Hyperloop's near-vacuum conditions, the study found that epoxy-coated concrete significantly reduced air permeability compared to uncoated concrete, with specimens coated on both sides approaching near-zero permeability.
View Article and Find Full Text PDFRev Sci Instrum
December 2024
Max-Planck-Insitut für Plasmaphysik, Boltzmannstrasse 2, Garching D-85748, Germany.
The Testbed for Analysis of Permeation of Atoms in Samples (TAPAS) is an experimental setup for ion-driven permeation studies with a focus on investigating wall materials for nuclear fusion devices. A monoenergetic, mass-filtered high-intensity keV ion beam is focused and directed onto the permeation sample by electrostatic ion optics and decelerated to the desired ion energy by a dedicated set of apertures close to the sample. We were able to obtain ion energies as low as 170 eV/D with a D3+ ion beam with an ion flux density of the order of 1020 D/m2s on a beam-wetted area of ∼33 mm2.
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