Two rare mixed-cluster-organic frameworks (CHNH)[Cu-(μ-O)(L)][MnMoO(L)]·4NMF·5HO (1) and [(CH)NH][Co-(μ-O)(L)]-[MnMoO(L)]·5DMF (2) (L = 2-(hydroxymethyl)-2-(pyridin-4-yl)-1,3-propanediol; L = 4-(2-(4-pyridyl)ethenyl) benzoic acid; NMF = N-methylformamide; DMF = N,N-dimethylformamide) have been obtained, exhibiting the first two porous materials simultaneously integrating polyoxometalates and transition-metal-oxygen clusters as secondary building units (SBUs).
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