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{Np} clusters: the missing link in the largest poly-oxo cluster series of tetravalent actinides. | LitMetric
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{Np} clusters: the missing link in the largest poly-oxo cluster series of tetravalent actinides.

Nicolas P Martin Christophe Volkringer Pascal Roussel Juliane März Christoph Hennig Thierry Loiseau Atsushi Ikeda-Ohno

Chem Commun (Camb)

Unité de Catalyse et Chimie du Solide (UCCS), UMR, CNRS 8181, Université de Lille, École Nationale Supérieure de Chimie de Lille Centrale Lille, Université Artois, Lille 59000, France.

Published: September 2018

Two poly-oxo cluster complexes of tetravalent neptunium (Np(iv)), Np38O56Cl18(bz)24(THF)8·nTHF and Np38O56Cl42(ipa)20·mipa (bz = benzoate, THF = tetrahydrofuran, and ipa = isopropanol), were obtained via solvothermal synthesis and structurally characterised by single-crystal X-ray diffraction. The {Np38} clusters are comparable to the analogous {U38} and {Pu38} motifs, filling the gap in this largest poly-oxo cluster series of tetravalent actinides.

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http://dx.doi.org/10.1039/c8cc03744bDOI Listing

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