This paper describes the synthesis and performance evaluation of a granular solid desiccant composite synthesized through a sol-gel process at atmospheric pressure and ambient temperature. The composite desiccant essentially comprises of a biopolymer template, chitosan, and nanoscale boehmite particles embedded on the fibrils of the biopolymer. The chitosan fibers not only help in the formation of boehmite nanoparticles but also act as a reinforcing agent and enable the formation of sand like granules upon aging and drying. The composite showed promising ability to dehumidify the moist air. The desiccant was characterized in detail to study its textural, morphological and chemical properties. The results revealed the formation of crystalline, nanostructured composite with moisture adsorption capacity more than its self-weight (>1.5 g/g at 55-65% RH). The high moisture removal capacity, ease of synthesis and scale-up, and green synthesize approach would make the material a sustainable substitute for silica gel.
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http://dx.doi.org/10.1016/j.carbpol.2018.04.051 | DOI Listing |
Zhongguo Zhong Yao Za Zhi
December 2024
Engineering Research Center for Industrialization of Southern Medicinal Plants Resources of Hainan Province, Hainan Normal University Haikou 571158, China Key Laboratory of Southern Medicinal Plants Resources of Haikou City, Hainan Normal University Haikou 571158, China Key Laboratory of Tropical Medicinal Resource Chemistry of Ministry of Education, Hainan Normal University Haikou 571158, China.
The chemical constituents from the stems and leaves of Mycetia hainanensis were isolated by silica gel, ODS gel, and Sephadex LH-20 gel column chromatography and preparative HPLC. The chemical structures of all the isolated compounds were identified on the basis of their physicochemical properties, spectroscopic data, as well as the comparison of their physicochemical and spectroscopic data with the reported data in literature. Twelve compounds were isolated from the 85% ethanol extract of the stems and leaves of M.
View Article and Find Full Text PDFSoft Matter
January 2025
Faculty of Science and Letters, Department of Chemistry, Soft Materials Research Laboratory, Istanbul Technical University, Istanbul, Maslak, 34469, Turkey.
A series of anionic poly(acrylamide--sodium acrylate)/poly(ethylene glycol), PAN/PEG, hybrids were conveniently synthesized free radical aqueous polymerization by integrating bentonite, kaolin, mica, graphene and silica, following a simple and eco-friendly crosslinking methodology. A comparative perspective was presented on how integrated nanofillers affect the physicochemical properties of hybrid gels depending on the differences in their structures. Among the five types of nanofillers, bentonite-integrated hybrid gel had the highest water absorbency, while graphene-integrated gel had the lowest.
View Article and Find Full Text PDFTurk J Pharm Sci
January 2025
University of Tlemcen, Faculty of Science, Department of Chemistry, Laboratory of Natural and Bioactive Substances, Tlemcen, Algeria.
Objectives: This study focused on the phytochemical, insecticidal, and bactericidal activities of Vahl, as well as molecular docking analysis of an acetylcholinesterase (AChE) inhibitor as a promising natural insecticide.
Materials And Methods: The leaves of were successively extracted with n-hexane, acetone, and methanol. Silica gel column chromatography of the methanol extract yielded compound 1.
Anal Chim Acta
February 2025
Key Laboratory of Molecular Medicine and Biotherapy, School of Life Science, Beijing Institute of Technology, No. 5 Zhongguancun South Street, Beijing, 100081, China. Electronic address:
Background: The metal organic cages (MOCs) are an emerging type of porous material that has attracted considerable research interest due to their unique properties, including good stability and well-defined intrinsic cavities. The chiral MOCs with porous structures have broad application prospects in enantiomeric recognition and separation. However, there are almost no relevant reports on chiral MOCs as chiral stationary phases (CSPs) for enantioseparation by high-performance liquid chromatography (HPLC).
View Article and Find Full Text PDFJ Ethnopharmacol
January 2025
State Key Laboratory of Medicinal Chemical Biology, College of Pharmacy and Tianjin Key Laboratory of Molecular Drug Research, Nankai University, Tianjin 300353, People's Republic of China. Electronic address:
Ethnopharmacological Relevance: The whole plant of Laggera alata is frequently utilize to remedy inflammatory diseases including nephritis as a traditional Chinese medicine. However, its active ingredients and mechanism of action against sepsis-associated acute kidney injury (SA-AKI) are unknown.
Aim Of The Study: This study aimed to identify active compounds from L.
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