Modern resolution-enhanced NMR techniques can monitor the in situ discrimination of co-existing isotropic and anisotropic contributions of small molecules dissolved in weakly aligning PMMA/CDCl3 media. The simultaneous sign-sensitive determination of accurate Δδ ( H), Δδ ( C) and/or isotropic J and anisotropic T coupling constants (and consequently H- C residual dipolar couplings and H/ C residual chemical shift anisotropies) can be performed from spectral-aliased heteronuclear single-quantum correlation spectra.
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| http://dx.doi.org/10.1002/cphc.201800094 | DOI Listing |
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