The aim of this study was to evaluate the degree of conversion (DC%), water sorption (WS), solubility (SO), and resin-dentin bonding stability of experimental adhesive systems containing ZnCl. Different concentrations (wt.%) of ZnCl were added to a model etch-and-rinse adhesive system consisting of BISGMA, HEMA, UDMA, GDMA, water, and ethanol: Zn0 (0%-control group); Zn2 (2%); Zn3.5 (3.5%); and Zn5 (5%). Adper Single Bond 2 (SB) was used as commercial reference. The samples were light cured for 20s using a quartz-tungsten-halogen unit (650 mW/cm). DC% ( = 5) was measured using FT-IR spectroscopy, and WS and SO ( = 5) were calculated based on ISO4049. Microtensile bond strength (TBS) and nanoleakage (NL) were measured after 24 h and 12 months of water storage ( = 10). Data were analyzed using ANOVA and Tukey's HSD test (5%). Zn5 presented the lowest DC% and the highest WS and SO ( < 0.05). Zn0 and Zn2 presented statistically similar DC%, WS, SO, and immediate TBS. All adhesives containing ZnCl maintained a TBS stability after 12 months, but only Zn2 and Zn3.5 did not suffer an increase in NL. SB presented the highest immediate TBS but the greatest reduction after 12 months ( < 0.05). The addition of 2 wt.% of ZnCl in adhesive formulations seems to be a promising way to improve the resin-dentin bonding stability. Higher concentrations than 2 wt.% could impair some physicochemical properties.
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http://dx.doi.org/10.1155/2017/5940479 | DOI Listing |
J Esthet Restor Dent
January 2025
Magne Education, Beverly Hills, California, USA.
Objective: Chemicals used during canal disinfection and endodontic sealers have a deleterious effect on dentin bond strength. The aim of this study was to evaluate a novel clinical sequence to improve the resin-dentin microtensile bond strength (μTBS) to endodontically treated teeth.
Materials And Methods: Twenty human molars were distributed in four experimental groups (n = 5, N = 20): C-control group without exposure to any endodontic chemical substances (2.
J Dent Res
December 2024
State Key Lab of Supramolecular Structure and Materials, College of Chemistry, Jilin University, Changchun, China.
The cross-linking reagent has been proposed as a means of modifying dentin collagen, inhibiting matrix metalloproteinase activities, and enhancing bond durability during dentin bonding procedures. This study aimed to synthesize an operation-friendly dual cross-linking reagent-3-(4-formyphenoxy)-2-hydroxypropyl methacrylate (FPA)-to assess its ability to cross-link dentin collagen and reduce enzymatic activity at the bonding interface. Cytotoxicity was evaluated by a cell counting kit-8 test and calcein AM/propidium iodide assay.
View Article and Find Full Text PDFHeliyon
December 2024
Department of Advanced General Dentistry, Faculty of Dentistry, Mahidol University, Bangkok, 10400, Thailand.
Objective: The purpose of this study was to examine the effect of several antiseptic mouthwashes on the dentin microtensile bond strength of self-etch adhesive, considering the influence of rinsing with water.
Methods: Forty flat dentin surfaces were produced by sectioning sound extracted third molars. They were randomly divided into four main groups: (1) artificial saliva (control); (2) 1 % hydrogen peroxide; (3) 0.
J Dent (Shiraz)
December 2024
Dept. Conservative Dentistry and Endodontics, St.Joseph Dental College, Duggirala, Eluru, Andra Pradesh, India.
Statement Of The Problem: Dentin bonding with etch-and-rinse adhesives involves demineralizing the 5-8µm of the surface dentin to create micro space for resin infiltration. The presence of continuous fluid movement in dentin tubules and positive pulpal pressure prevents complete water replacement by resin monomers. This results in areas of demineralized dentin, which contain collagen fibers without resin infiltration.
View Article and Find Full Text PDFBMC Oral Health
November 2024
Department of Restorative Dentistry, Faculty of Dentistry, King Abdulaziz University, Jeddah, Saudi Arabia.
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