An efficient synthesis of unsolvated KBH was achieved by the reaction of a liquid K-Na alloy with BH·THF at room temperature. KBH was found to release hydrogen and minor boranes by subsequent cleavage of its B-H and B-H-B bonds during pyrolysis, and yield KBH as a major product.
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| http://dx.doi.org/10.1039/c7cc06414d | DOI Listing |
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