The structure of one of the first permanently porous metal phosphonates, MIL-91(Al) was re-determined using high resolution synchrotron powder X-ray diffraction data. The new model is in a lower symmetry space group, with no disordered ligands in the structure, whilst remaining otherwise consistent with the reported compound. New milder synthetic conditions were also developed.
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| http://www.ncbi.nlm.nih.gov/pmc/articles/PMC5324569 | PMC |
| http://dx.doi.org/10.1002/zaac.201600358 | DOI Listing |
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