Preparation of Er:YAlO/WO-KNbO composite and application in treatment of methamphetamine under ultrasonic irradiation.

Ultrason Sonochem

College of Chemistry, Liaoning University, Shenyang 110036, PR China; College of Environment, Liaoning University, Shenyang 110036, PR China. Electronic address:

Published: March 2017

Er:YAlO/WO-KNbO composite powder as an effective sonocatalyst was prepared via collosol-gelling-hydrothermal and high-temperature calcination methods. The textures of materials were observed by X-ray diffractometer (XRD), scanning electron microscopy (SEM) and X-ray photoelectron spectroscopy (XPS). In order to estimate the sonocatalytic activity of Er:YAlO/WO-KNbO composite powder, the sonocatalytic degradation of methamphetamine (MAPA) was performed. Furthermore, the influences of mass ratio of WO and KNbO, ultrasonic irradiation time, catalyst addition amount, initial methamphetamine (MAPA) concentration and used times on the sonocatalytic degradation of methamphetamine (MAPA) caused by Er:YAlO/WO-KNbO composite powder were investigated by using gas chromatography. Under optimal conditions of 1.00g/L Er:YAlO/WO-KNbO addition amount and 10.00mg/L methamphetamine (MAPA) initial concentration, 68% of methamphetamine (MAPA) could be removed after 150min ultrasonic irradiation. The experimental results showed that the Er:YAlO/WO-KNbO as sonocatalyst displayed an excellent sonocatalytic activity in degradation of methamphetamine (MAPA) under ultrasonic irradiation.

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http://dx.doi.org/10.1016/j.ultsonch.2016.11.004DOI Listing

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