A single-step, self-contained method for determining the crystallite-size distribution and shape from experimental x-ray line profile data is presented. It is shown that the crystallite-size distribution can be determined without invoking a functional form for the size distribution, determining instead the size distribution with the least assumptions by applying the Bayesian/MaxEnt method. The Bayesian/MaxEnt method is tested using both simulated and experimental CeO2 data, the results comparing favourably with experimental CeO2 data from TEM measurements.
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| http://www.ncbi.nlm.nih.gov/pmc/articles/PMC4849618 | PMC |
| http://dx.doi.org/10.6028/jres.109.012 | DOI Listing |
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