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Putting chromium on the map for N2 reduction: production of hydrazine and ammonia. A study of cis-M(N2)2 (M = Cr, Mo, W) bis(diphosphine) complexes. | LitMetric
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Putting chromium on the map for N2 reduction: production of hydrazine and ammonia. A study of cis-M(N2)2 (M = Cr, Mo, W) bis(diphosphine) complexes.

Jonathan D Egbert Molly O'Hagan Eric S Wiedner R Morris Bullock Nicholas A Piro W Scott Kassel Michael T Mock

Chem Commun (Camb)

Center for Molecular Electrocatalysis, Pacific Northwest National Laboratory, P.O. Box 999, K2-57, Richland, WA 99352, USA.

Published: July 2016

The first complete structurally and spectroscopically characterized series of isostructural Group 6 N2 complexes is reported. Protonolysis experiments on cis-[M(N2)2(P(Et)N(R)P(Et))2] (M = Cr, Mo, W; R = 2,6-difluorobenzyl) reveal that only Cr affords N2H5(+) and NH4(+) from the reduction of the N2 ligands.

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http://dx.doi.org/10.1039/c6cc03449gDOI Listing

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