A compact retarding field analyzer with embedded quartz crystal microbalance has been developed to measure deposition rate, ionized flux fraction, and ion energy distribution arriving at the substrate location. The sensor can be placed on grounded, electrically floating, or radio frequency (rf) biased electrodes. A calibration method is presented to compensate for temperature effects in the quartz crystal. The metal deposition rate, metal ionization fraction, and energy distribution of the ions arriving at the substrate location are investigated in an asymmetric bipolar pulsed dc magnetron sputtering reactor under grounded, floating, and rf biased conditions. The diagnostic presented in this research work does not suffer from complications caused by water cooling arrangements to maintain constant temperature and is an attractive technique for characterizing a thin film deposition system.

Download full-text PDF

Source
http://dx.doi.org/10.1063/1.4946788DOI Listing

Publication Analysis

Top Keywords

deposition rate
12
energy distribution
12
quartz crystal
12
ion energy
8
pulsed magnetron
8
magnetron sputtering
8
retarding field
8
field analyzer
8
analyzer embedded
8
embedded quartz
8

Similar Publications

Pulsed-Current Operation Enhances HO Production on a Boron-Doped Diamond Mesh Anode in a Zero-Gap PEM Electrolyzer.

ChemSusChem

January 2025

Department of Chemical Engineering, MESA+ Institute for Nanotechnology, Faculty of Science and Technology, University of Twente, Drienerlolaan 5, 7522 NB, Enschede, The, Netherlands.

A niobium (Nb) mesh electrode was coated with boron-doped diamond (BDD) using chemical vapor deposition in a custom-built hot-filament reactor. The BDD-functionalized mesh was tested in a zero-gap electrolysis configuration and evaluated for the anodic formation of HO by selective oxidation of water, including the analysis of the effects on Faradaic efficiency towards HO (FEH2O2) induced by pulsed electrolysis. A low electrolyte flow rate (V⋅) was found to result in a relatively high concentration of HO in single-pass electrolysis experiments.

View Article and Find Full Text PDF

Atmospheric Deposition of Microplastics in South Central Appalachia in the United States.

ACS EST Air

January 2025

Department of Civil and Environmental Engineering, Virginia Tech, Blacksburg, Virginia 24061, United States.

Due to the increased prevalence of plastic pollution globally, atmospheric deposition of microplastics (MPs) is a significant issue that needs to be better understood to identify potential consequences for human health. This study is the first to quantify and characterize atmospheric MP deposition in the Eastern United States. Passive sampling was conducted at two locations within the Eastern United States, specifically in remote South Central Appalachia, from March to September 2023.

View Article and Find Full Text PDF

A Multifunctional Synergistic Solar-Driven Interfacial Evaporator for Desalination and Photocatalytic Degradation.

ACS Appl Mater Interfaces

January 2025

State Key Laboratory of Silicate Materials for Architectures, Wuhan University of Technology, Wuhan 430070, P. R. China.

The scarcity of freshwater resources and the treatment of dye wastewater have emerged as unavoidable challenges that need to be addressed. The combination of solar-driven interfacial evaporation, photocatalytic degradation, and superhydrophobic surface provides an effective approach for seawater desalination and the treatment of organic dyes. In this study, we fabricated a multifunctional synergistic solar evaporator by depositing cupric oxide nanoparticles onto polypyrrole (PPy) coating and subsequently modified it with a hydrophobic agent successfully.

View Article and Find Full Text PDF

Platelet-derived extracellular vesicles (PEVs) are rich in growth factors and have significant potential for facilitating tissue repair and regeneration. Therefore, we conducted this meta-analysis to assess the efficacy of PEVs in treating diabetic wounds. To assess the efficacy and safety of PEVs in treating diabetic wounds, we conducted a systematic review of several databases and performed a meta-analysis using a random effects model.

View Article and Find Full Text PDF

Tailoring selenization dynamics: How heating rate manipulates nucleation and growth boosts efficiency in kesterite solar cells.

J Chem Phys

January 2025

Institute of Photoelectronic Thin Film Devices and Technology, Tianjin Key Laboratory of Thin Film Devices and Technology, Nankai University, Tianjin 300350, China.

Kesterite Cu2ZnSn(S,Se)4 (CZTSSe) has emerged as a promising photovoltaic material due to its low cost and high stability. The CZTSSe film for high-performance solar cells can be obtained by annealing the deposited CZTS precursor films with selenium (a process known as selenization). The design of the selenization process significantly affects the quality of the absorber layer.

View Article and Find Full Text PDF

Want AI Summaries of new PubMed Abstracts delivered to your In-box?

Enter search terms and have AI summaries delivered each week - change queries or unsubscribe any time!