Analysis of small-angle X-ray scattering data in the presence of significant instrumental smearing.

J Appl Crystallogr

Division of Physical Chemistry, Center of Chemistry and Chemical Engineering, Lund University, SE-221 00 Lund, Sweden.

Published: February 2016

A laboratory-scale small-angle X-ray scattering instrument with pinhole collimation has been used to assess smearing effects due to instrumental resolution. A new, numerically efficient method to smear ideal model intensities is developed and presented. It allows for directly using measured profiles of isotropic but otherwise arbitrary beams in smearing calculations. Samples of low-polydispersity polymer spheres have been used to show that scattering data can in this way be quantitatively modeled even when there is substantial distortion due to instrumental resolution.

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http://www.ncbi.nlm.nih.gov/pmc/articles/PMC4762572PMC
http://dx.doi.org/10.1107/S1600576715023444DOI Listing

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