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Little information exists on the effects of ensiling on condensed tannins or proanthocyanidins. The acetone-butanol-HCl assay is suitable for measuring proanthocyanidin contents in a wide range of samples, silages included, but provides limited information on proanthocyanidin composition, which is of interest for deciphering the relationships between tannins and their bioactivities in terms of animal nutrition or health. Degradation with benzyl mercaptan (thiolysis) provides information on proanthocyanidin composition, but proanthocyanidins in several sainfoin silages have proved resistant to thiolysis. We now report that a pretreatment step with sodium hydroxide prior to thiolysis was needed to enable their analysis. This alkaline treatment increased their extractability from ensiled sainfoin and facilitated especially the release of larger proanthocyanidins. Ensiling reduced assayable proanthocyanidins by 29%, but the composition of the remaining proanthocyanidins in silage resembled that of the fresh plants.
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http://dx.doi.org/10.1021/acs.jafc.5b04106 | DOI Listing |
Shanghai Kou Qiang Yi Xue
October 2024
Department of General Dentistry, Shanghai Ninth People's Hospital, Shanghai Jiao Tong University School of Medicine; College of Stomatology, Shanghai Jiao Tong University; National Center for Stomatology; National Clinical Research Center for Oral Diseases; Shanghai Key Laboratory of Stomatology; Shanghai Research Institute of Stomatology. Shanghai 200011, China. E-mail:
Purpose: To evaluate the efficacy of micro-computed tomography(Micro-CT) in removing calcium hydroxide from posterior curved root canals.
Methods: Twenty molar teeth (48 root canals) extracted at the Department of General Dentistry, Shanghai Ninth People's Hospital between December 2023 and February 2024 were collected. After preparing by Ni-TI instruments M3 according to standard root canal treatment procedures, calcium hydroxide was injected into the root canals.
Int J Biol Macromol
December 2024
College of Environmental and Biological Engineering, Putian University, No. 1133 Middle Xueyuan Street, Chengxiang District, Putian City, Fujian Province 351100, People's Republic of China; Fujian Provincial Key Laboratory of Ecology-Toxicological Effects & Control for Emerging Contaminants, Putian University, No. 1133 Middle Xueyuan Street, Chengxiang District, Putian City, Fujian Province 351100, People's Republic of China; Key Laboratory of Ecological Environment and Information Atlas, Putian University, No. 1133 Middle Xueyuan Street, Chengxiang District, Putian City, Fujian Province 351100, People's Republic of China.
Applying cellulose paper on the triboelectric material is the trend of developing eco-friendly triboelectric nanogenerator (TENG). However, the researchers always pay attention to improve the triboelectric property of cellulose paper by the grafting of functional groups and the introduction of conductive or high dielectric property materials, while neglecting the effects of lignocellulose fiber composition including hemicellulose and lignin. In this work, the contents of hemicellulose and lignin were adjusted by sodium hydroxide and sodium chlorite, respectively; and the effects of hemicellulose and lignin on the triboelectric performance of cellulose paper were evaluated.
View Article and Find Full Text PDFACS Omega
December 2024
Key Laboratory for Enhanced Oil & Gas Recovery of the Ministry of Education, Northeast Petroleum University, Daqing 163318, Heilongjiang, China.
In alkali/surfactant/polymer (ASP) flooding systems, alkalis react with clay minerals such as Illite, montmorillonite, and kaolinite, leading to reservoir damage and impacting oil recovery rates. Therefore, studying the dissolution effects of strong alkalis on clay minerals is crucial for improving oil recovery. This study uses Illite as a representative clay mineral and employs the ReaxFF reactive force field and molecular dynamics simulations to model its dissolution in NaOH solution.
View Article and Find Full Text PDFJ Biomater Sci Polym Ed
December 2024
Polymeric Biomaterials Lab, School of Nanosciences and Molecular Medicine, Amrita Vishwa Vidyapeetham, Kochi, India.
Chitin hydrogel and hydrogel-based products are some of the frequently reported biomaterials for biomedical applications. Yet there is a void in understanding chitin's dissolution mechanism and its most suitable solvent system(s). Chitin is a natural polysaccharide polymer which can be dissolved in solvents such as calcium chloride- methanol, sodium hydroxide/urea (NaOH/urea), lithium chloride diacetamide (LiCl/DMAc), ionic liquids and deep eutectic solvents.
View Article and Find Full Text PDFInt J Ophthalmol
December 2024
Xiamen University Affiliated Xiamen Eye Center, Eye Institute of Xiamen University, School of Medicine, Xiamen University, Xiamen 3611002, Fujian Province, China.
Aim: To establish a stable, short-time, low-cost and reliable murine model of meibomian gland dysfunction (MGD).
Methods: A filter paper sheet soaked in 1.0 mol/L sodium hydroxide (NaOH) solution was used to touch the eyelid margin of C57BL/6J mice for 10s to establish the model.
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