We demonstrate the ability to apply electron energy loss spectroscopy (EELS) to follow the chemistry and oxidation states of LiMn2O4 and Li4Ti5O12 battery electrodes within a battery solvent. This is significant as the use and importance of in situ electrochemical cells coupled with a scanning/transmission electron microscope (S/TEM) has expanded and been applied to follow changes in battery chemistry during electrochemical cycling. We discuss experimental parameters that influence measurement sensitivity and provide a framework to apply this important analytical method to future in situ electrochemical studies.
Download full-text PDF |
Source |
|---|---|
| http://dx.doi.org/10.1039/c5cc07180a | DOI Listing |
Publication Analysis
Top Keywords
battery chemistry
8
electron energy
8
energy loss
8
loss spectroscopy
8
situ electrochemical
8
probing battery
4
chemistry liquid
4
liquid cell
4
cell electron
4
spectroscopy demonstrate
4
Similar Publications
Want AI Summaries of new PubMed Abstracts delivered to your In-box?
Enter search terms and have AI summaries delivered each week - change queries or unsubscribe any time!