Air oxidative radical oxysulfurization of alkynes initiated by 0.5 mol % tert-butyl hydroperoxide with arylthiols is described. The reaction proceeded at room temperature in the presence of 5% mol water to afford selective α-thioaldehydes.
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| http://dx.doi.org/10.1021/acs.joc.5b00641 | DOI Listing |
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