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Cationic Coordination Modification Drives Birefringence and Nonlinear Effect Double Lifting in Sulfate.
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Guangxi Key Laboratory of Electrochemical Energy Materials, School of Chemistry and Chemical Engineering, Guangxi University, Nanning, Guangxi 530004, China.
As nonlinear optical (NLO) crystals, sulfates have the superiority of transparency for ultraviolet (UV) light, but they are often troubled by small nonlinear coefficients and birefringence owing to the high symmetry of the [SO] group. By introducing two neutral diethylenetriamine (DETA) molecules to replace the six coordinated water molecules of the [Zn(HO)] complex cation in [Zn(HO)](SO)(HO), a new sulfate with an acentric structure, namely, [Zn(DETA)](SO)(HO), has been designed and synthesized. Structural investigation reveals that the coordination modification of Zn ion tremendously enhances its intraoctahedral distortion.
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