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A new stability indicating HPLC method with QDa and PDA detectors for the determination of process and degradation impurities of ivabradine including separation of diastereomeric -oxides.
Anal Methods
January 2025
Istanbul University, Faculty of Pharmacy, Department of Analytical Chemistry, 34116, Istanbul, Turkey.
In this study, a new reversed phase high performance liquid chromatography method using two detectors was developed for the analysis of degradation and process impurities of ivabradine in pharmaceutical preparations. A PDA detector set to 285 nm wavelength and a QDa detector set to positive scan mode were used in the method. In the developed method, the separation process was carried out in a Zorbax phenyl column with a gradient application of a 0.
View Article and Find Full Text PDFPurification immunoglobulin yolk anti avian influenza H5N1 in poultry using hydrophobic interaction chromatography.
Poult Sci
January 2025
Research Center for Molecular Biotechnology and Bioinformatics, Universitas Padjadjaran, West Java, 40132, Indonesia; Faculty of Pharmacy, Universitas Bhakti Kencana, West Java, 40614, Indonesia.
Avian influenza is a significant threat to the poultry industry, and it has become an outbreak in many countries because of its mortality and morbidity. Concerns about the history of avian influenza outbreaks has prompted all countries to enhance their independence in pharmaceutical and biological components as a preparedness measure for any potential occurrences. The production of antibodies such as IgY is a potential alternative.
View Article and Find Full Text PDFThe Effects of a Blend of Essential Oils in the Milk of Suckling Calves on Performance, Immune and Antioxidant Systems, and Intestinal Microbiota.
Animals (Basel)
December 2024
Department of Animal Science, Universidade do Estado de Santa Catarina (UDESC), Chapecó 89815-630, SC, Brazil.
The objective of the present study was to determine whether the addition of a blend based on the essential oils of cinnamon, oregano, and eucalyptus to the liquid diets of calves would stimulate the immune system combined with anti-inflammatory action, minimize oxidative responses, and alter the intestinal microbiota, consequently enhancing animal growth. Twenty-four male Holstein calves (approximately five days old) were suckled for 60 days, underwent a weaning process, and were followed up until day 75 of the experiment. The calves were divided into control ( = 12) and phytobiotic ( = 12) groups, receiving commercial milk replacer and pelleted concentrate ad libitum.
View Article and Find Full Text PDFInvestigation of Filtration Performances in Eggshell Ultrafiltration Membranes with Surface Functionalized Using Graphene Oxide.
ACS Omega
December 2024
Department of Physics, Faculty of Mathematics and Natural Science, Universitas Padjadjaran, Jalan Raya Bandung-Sumedang Km 21 Jatinangor, Sumedang 45363, Indonesia.
Article Synopsis
- This study highlights the significance of preventing fouling in ultrafiltration membranes to improve their efficiency in wastewater treatment, particularly for dissolved dye molecules.
- Researchers tested eggshell membranes modified with different concentrations of graphene oxide (GO) to assess impacts on permeability, rejection efficiency, and flow rates.
- The findings demonstrate that the optimal use of 0.5 mg/mL GO at 45 psi pressure significantly enhances membrane performance, achieving a rejection efficiency of 36.6% and improving the filtration process's effectiveness against dye concentration.
Factors influencing oocyte recovery during ultrasound-guided follicle aspiration in mares: A postmortem study.
Theriogenology
December 2024
Equine Fertility Group, Facultad de Veterinaria, Universidad Cardenal Herrera-CEU, CEU Universities, Alfara Del Patriarca, Spain. Electronic address:
The objectives of this study were to investigate the influence of different OPU variables (vacuum and injection pressures during follicle aspiration and flushing, needle twisting to scrape follicles, number of follicle flushes and type of flushing media) on oocyte recovery rate (ORR) and morphology. Overall, 120 postmortem excised ovaries were processed in 62 replicates (1.9 ± 0.
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