The assessment of selectivity in different Quadrupole-Orbitrap mass spectrometry acquisition modes.

J Am Soc Mass Spectrom

RIKILT, Wageningen UR, Akkermaalsbos 2, 6708WB, P.O. Box 230, 6700AE, Wageningen, The Netherlands,

Published: February 2015

AI Article Synopsis

  • The study evaluated selectivity in liquid chromatography-tandem mass spectrometry (LC-MS/MS) with Q-Orbitrap by analyzing 108 samples, utilizing different acquisition modes like full scan, all ion fragmentation, and product ion scanning.
  • It employed reconstructed ion chromatograms and simulated selected reaction monitoring (SRM) to compare the effectiveness of various methods while performing an Analysis of Variance to identify significant factors affecting selectivity, including mass resolution and compound characteristics.
  • Results indicated that precursor ion selection is crucial for selectivity, with high accuracy monitoring of single product ions performing similarly or better than traditional methods, suggesting a need for updated identification standards in residue analysis and sports doping.

Article Abstract

Selectivity of the confirmation of identity in liquid chromatography (tandem) mass spectrometry using Q-Orbitrap instrumentation was assessed using different acquisition modes based on a representative experimental data set constructed from 108 samples, including six different matrix extracts and containing over 100 analytes each. Single stage full scan, all ion fragmentation, and product ion scanning were applied. By generating reconstructed ion chromatograms using unit mass window in targeted MS(2), selected reaction monitoring (SRM), regularly applied using triple-quadrupole instruments, was mimicked. This facilitated the comparison of single stage full scan, all ion fragmentation, (mimicked) SRM, and product ion scanning applying a mass window down to 1 ppm. Single factor Analysis of Variance was carried out on the variance (s(2)) of the mass error to determine which factors and interactions are significant parameters with respect to selectivity. We conclude that selectivity is related to the target compound (mainly the mass defect), the matrix, sample clean-up, concentration, and mass resolution. Selectivity of the different instrumental configurations was quantified by counting the number of interfering peaks observed in the chromatograms. We conclude that precursor ion selection significantly contributes to selectivity: monitoring of a single product ion at high mass accuracy with a 1 Da precursor ion window proved to be equally selective or better to monitoring two transition products in mimicked SRM. In contrast, monitoring a single fragment in all ion fragmentation mode results in significantly lower selectivity versus mimicked SRM. After a thorough inter-laboratory evaluation study, the results of this study can be used for a critical reassessment of the current identification points system and contribute to the next generation of evidence-based and robust performance criteria in residue analysis and sports doping.

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http://dx.doi.org/10.1007/s13361-014-1021-xDOI Listing

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