Ink dating using thermal desorption and gas chromatography/mass spectrometry: comparison of results obtained in two laboratories.

J Forensic Sci

Ecole des Sciences Criminelles, Institut de Police Scientifique, University of Lausanne, Bâtiment Batochime, 1015, Lausanne-Dorigny, Switzerland; Bundeskriminalamt, Forensic Science Institute, 651, Wiesbaden, Germany.

Published: January 2015

An ink dating method based on solvent analysis was recently developed using thermal desorption followed by gas chromatography/mass spectrometry (GC/MS) and is currently implemented in several forensic laboratories. The main aims of this work were to implement this method in a new laboratory to evaluate whether results were comparable at three levels: (i) validation criteria, (ii) aging curves, and (iii) results interpretation. While the results were indeed comparable in terms of validation, the method proved to be very sensitive to maintenances. Moreover, the aging curves were influenced by ink composition, as well as storage conditions (particularly when the samples were not stored in "normal" room conditions). Finally, as current interpretation models showed limitations, an alternative model based on slope calculation was proposed. However, in the future, a probabilistic approach may represent a better solution to deal with ink sample inhomogeneity.

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http://dx.doi.org/10.1111/1556-4029.12603DOI Listing

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