Quick re-introduction of selective scalar interactions in a pure-shift NMR spectrum.

Chem Commun (Camb)

NMR Research Centre and Solid State and Structural Chemistry Unit, Indian Institute of Science, Bangalore 560012, India.

Published: December 2014

A new 1D NMR experiment cited as 'Quick G-SERF', which re-introduces selective proton-proton scalar interactions in a pure shift spectrum during real time data acquisition, is reported. The method provides information on multiple proton-proton couplings from a single experiment, analogous to the 2D G-SERF technique, while significantly shortening the experimental time by 1-2 orders of magnitude due to reduced dimension and enhanced sensitivity.

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http://dx.doi.org/10.1039/c4cc06772jDOI Listing

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