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Crystal structure of 1-meth-oxy-2,2,2-tris-(pyrazol-1-yl)ethane. | LitMetric

Crystal structure of 1-meth-oxy-2,2,2-tris-(pyrazol-1-yl)ethane.

Acta Crystallogr Sect E Struct Rep Online

Department of Biochemistry and Chemistry, Southern Arkansas University, Magnolia, AR 71753, USA.

Published: September 2014

The title compound, C12H14N6O, consists of three pyrazole rings bound via nitro-gen to the distal ethane carbon of meth-oxy ethane. The dihedral angles between the three pyrazole rings are 67.62 (14), 73.74 (14), and 78.92 (12)°. In the crystal, mol-ecules are linked by bifurcated C-H,H⋯N hydrogen bonds, forming double-stranded chains along [001]. The chains are linked via C-H⋯O hydrogen bonds, forming a three-dimensional framework structure. The crystal was refined as a perfect (0.5:0.5) inversion twin.

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Source
http://www.ncbi.nlm.nih.gov/pmc/articles/PMC4186097PMC
http://dx.doi.org/10.1107/S1600536814018789DOI Listing

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