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(Benzyl-diphenyl-phosphane-1κP)[μ-bis(diphenylphosphan-yl)methane-2:3κ(2) P:P']nona-carbonyl-1κ(3) C,2κ(3) C,3κ(3) C-triangulo-triruthenium(0). | LitMetric
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(Benzyl-diphenyl-phosphane-1κP)[μ-bis(diphenylphosphan-yl)methane-2:3κ(2) P:P']nona-carbonyl-1κ(3) C,2κ(3) C,3κ(3) C-triangulo-triruthenium(0).

Omar Bin Shawkataly Imthyaz Ahmed Khan Siti Syaida Sirat Mohd Mustaqim Rosli

Acta Crystallogr Sect E Struct Rep Online

X-Ray Crystallography Unit, School of Physics, Universiti Sains Malaysia, 11800 USM, Penang, Malaysia.

Published: August 2014

The asymmetric unit of the title compound, [Ru3(C19H17P)(C25H22P2)(CO)9], consists of two independent mol-ecules. The bis-(di-phenyl-phosphan-yl)methane ligand bridges an Ru-Ru bond and the benzyl-diphenyl-phosphane ligand binds to the third Ru atom. The Ru-Ru bond cis to the benzyl-diphenyl-phosphane ligand is the longest of the three Ru-Ru bonds in both mol-ecules. In the crystal, mol-ecules are linked by C-H⋯O hydrogen bonds, forming layers parallel to the ac plane. C-H⋯π contacts further stabilize the crystal packing.

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 Source
http://www.ncbi.nlm.nih.gov/pmc/articles/PMC4158507PMC
http://dx.doi.org/10.1107/S1600536814015475DOI Listing

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