A simple, fast, efficient and eco-friendly procedure was developed for the synthesis of alkyl and aryl-N-methylnitrones. The corresponding nitrones of aromatic aldehydes, aliphatic aldehydes and alicyclic carbonyl compounds were prepared from N-methylhydroxylamine hydrochloride and Na2CO3-Na2SO4 by simply grinding at room temperature without using solvent.
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| http://www.ncbi.nlm.nih.gov/pmc/articles/PMC6264226 | PMC |
| http://dx.doi.org/10.3390/molecules16086677 | DOI Listing |
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