Nanocrystalline cellulose (NCC) was prepared from microcrystalline cellulose (MCC) with particle size of 24.7 μm using sulfuric acid hydrolysis technique. The obtained NCC revealed size of 0-100 nm, which the major part of them was about 30 nm. Then different contents (2.5, 5 and 10 wt%) of these NCC incorporated in agar film solution and the morphology, structure, and properties of the nanocomposite films were characterized by scanning electron microscope (SEM), X-ray diffraction (XRD), Fourier transforms infrared (FTIR) spectroscopy, differential scanning calorimetry (DSC), mechanical, physical and optical testing. Results showed that the water vapor permeability (WVP) and water solubility (WS) of the agar-based nanocomposite films significantly (P<0.05) decreased about 13% and 21%, respectively, upon increasing the NCC content to 10%. Tensile strength (TS) and Young's modulus (YM) values of nanocomposite films significantly increased (P≤0.05) with addition of NCC, whereas the elongation percent (E%) decreased not significantly (P>0.05). In addition, swelling percentage, transparency and light transmission of the films were decreased by incorporating NCC into polymer matrix.
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http://dx.doi.org/10.1016/j.ijbiomac.2014.07.013 | DOI Listing |
Int J Biol Macromol
December 2021
Department of Food and Nutrition, BioNanocomposite Research Center, Kyung Hee University, 26 Kyungheedae-ro, Dongdaemun-gu, Seoul 02447, Republic of Korea. Electronic address:
A functional carrageenan/agar-based film was prepared by combining tea tree oil Pickering emulsion (PET) and zinc sulfide nanoparticles (ZnSNP). PET was formulated using tea tree essential oil stabilized with nanocellulose fibers. PET and ZnSNPs were uniformly dispersed in the binary polymer matrix and formed compatible films.
View Article and Find Full Text PDFInt J Biol Macromol
November 2021
Department of Fiber System Engineering, Yeungnam University, South Korea. Electronic address:
Synergistic combinations of pullulan, agar, montmorillonite (MMT) clay, and quaternary ammonium silane (QAS)-based (Pullulan/agar/MMT clay/QAS) active nanocomposites were prepared by a simple, cost-effective method. The Pullulan/agar/MMT clay/QAS nanocomposites were studied via Fourier-transform infrared spectroscopy, scanning electron microscopy, and X-ray diffraction analyses. The concentration of MMT clay played a very important role in the properties of the nanocomposites.
View Article and Find Full Text PDFColloids Surf B Biointerfaces
November 2021
Department of Food and Nutrition, BioNanocomposite Research Center, Kyung Hee University, 26 Kyungheedae-ro, Dongdaemun-gu, Seoul, 02447, Republic of Korea. Electronic address:
Here we report on the robust synthesis of zinc sulfide nanoparticles (ZnSNP) using a simple one-pot reaction. The prepared ZnSNP was characterized and confirmed to be a petal-shaped nanoparticle. The ZnSNP was added to fabricate the pectin/agar-based functional composite film.
View Article and Find Full Text PDFIran J Biotechnol
January 2021
Department of Chemistry, Faculty of Science, Kerman Branch, Islamic Azad University, Kerman, Iran.
Background: ZnO nanoparticles (ZnO-NPs) are one of the most popular metal oxide nanoparticles, which exhibit significant antibacterial properties against various pathogens. Among nanoparticle synthesis methods, the green synthesis using plant extract is considered as an eco-friendly and cost-effective method for ZnO-NPs production, compared to the chemical procedures.
Background: This study aimed to evaluate the green synthesis of ZnO-NPs loaded on silica gel matrix (ZnO/SG nanocomposite) by using methanol leaf extract of as a new extract and a cost-effective method.
Curr Pharm Des
June 2020
Department of Chemical Engineering, Dhofar University, Salalah, Oman.
Purpose: The purpose of the present study was to make a biocompatible agar based composite material via incorporation of appropriate additives within the agar matrix for potential applications in drug delivery and biomedical fields.
Methodology: Agar based composites were prepared by the incorporation of magnetic iron oxide nano particles, graphite and sodium aluminum as additives in different proportions within the agar matrix by a simple thermophysico- mechanical method. The as prepared agar based composites were then characterized by different techniques i.
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