Purpose: While it has been shown that no method produces specimens with exactly the same cross-sectional bonded area (BA), BA variations within and between studies are a well-known covariate in microtensile test results. However, no method has yet been described to accurately account for its influence. A procedure is presented that allows controlling for variations of BA effects on results. Further, a proposal for reporting is presented which enables results of different studies to be compared.
Materials And Methods: Partially using the results of the report in which the microtensile test was originally described, 144 both general (caused by differences in BA) and specific (due to a material's performance differences and intrinsic biological variability of specimens) variabilities were separated through linear regression of microtensile (MPa) to BA (mm2) pooled results. Comparing the specific variability of specimens - the residuals to the regression line - of groups allowed assessing differences between groups.
Results: A means comparison of residuals showed that specific differences were significant (t-test, p = 0.0004). The null hypothesis could be rejected: materials' performances were different. This could not be determined in the original report, since BA variability was very high. A proposal for reporting of results to facilitate their clinical interpretation and comparison between studies is presented.
Conclusion: Controlling for general variability caused by differences in BA size allows precise comparison of microtensile tests results.
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http://dx.doi.org/10.3290/j.jad.a32068 | DOI Listing |
Braz Oral Res
January 2025
Universidade de São Paulo - USP, School of Dentistry, Department of Operative Dentistry, São Paulo, SP, Brazil.
The aim of this study was to assess the effect of a chlorhexidine digluconate solution (CHX) applied as an antiproteolytic agent for controlling erosive tooth wear or as part of the adhesive treatment on long-term bond strength to eroded dentin. Dentin specimens were abraded with a 600-grit silicon carbide (SiC) paper for 1 min (sound dentin - S), subsequently treated with 2% CHX for 1 min (with excess removed, followed by a 6-hour rest), and eroded by exposure to Coca-Cola for 5 min, three times a day, for 5 days (CHX-treated and eroded dentin - CHXE), or only eroded (eroded dentin - E). The specimens were acid-etched (15 s), rinsed (30 s), dried (15 s), and rehydrated with 1.
View Article and Find Full Text PDFJ Esthet Restor Dent
January 2025
Magne Education, Beverly Hills, California, USA.
Objective: Chemicals used during canal disinfection and endodontic sealers have a deleterious effect on dentin bond strength. The aim of this study was to evaluate a novel clinical sequence to improve the resin-dentin microtensile bond strength (μTBS) to endodontically treated teeth.
Materials And Methods: Twenty human molars were distributed in four experimental groups (n = 5, N = 20): C-control group without exposure to any endodontic chemical substances (2.
Sci Rep
January 2025
Department of Materials Science and Engineering, Faculty of Mechanical Engineering, Budapest University of Technology and Economics, Műegyetem rkp. 3, Budapest, H-1111, Hungary.
Tooth degradation develops easily over time from initial caries to deeper cavities. The quality and durability of restorations are crucial in a patients' life, and it is primarily determined by the mechanical properties of the restorations. Clinicians and engineers apply biomimetic science in dentistry to mimic the natural design of the teeth and emphasize careful material selection as well as bond strength between the tissue and artificial material.
View Article and Find Full Text PDFJ Dent Res
December 2024
State Key Lab of Supramolecular Structure and Materials, College of Chemistry, Jilin University, Changchun, China.
The cross-linking reagent has been proposed as a means of modifying dentin collagen, inhibiting matrix metalloproteinase activities, and enhancing bond durability during dentin bonding procedures. This study aimed to synthesize an operation-friendly dual cross-linking reagent-3-(4-formyphenoxy)-2-hydroxypropyl methacrylate (FPA)-to assess its ability to cross-link dentin collagen and reduce enzymatic activity at the bonding interface. Cytotoxicity was evaluated by a cell counting kit-8 test and calcein AM/propidium iodide assay.
View Article and Find Full Text PDFBraz Dent J
December 2024
Department of Restorative Dentistry. Piracicaba Dental School, University of Campinas, Brazil.
This study investigated the effects of nonthermal atmospheric pressure plasma (NAPP) application and dentin rehydration with water (REHY) on bond strength (BS) of adhesives. Three etch-and-rinse adhesives were tested: Scotchbond Multi-Purpose (SBM / water-based primer + adhesive resin), Gluma Bond Universal (GBU / single-bottle containing acetone as organic solvent) and Prime&Bond Universal (PBU / single-bottle containing propanol as organic solvent). Adhesives were applied: 1- to phosphoric acid-etched dentin (Control), 2- after NAPP application for 45 seconds to etched dentin or 3- after REHY with water (10 seconds) of plasma-treated etched dentin.
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