A PHP Error was encountered

Severity: Warning

Message: file_get_contents(https://...@pubfacts.com&api_key=b8daa3ad693db53b1410957c26c9a51b4908&a=1): Failed to open stream: HTTP request failed! HTTP/1.1 429 Too Many Requests

Filename: helpers/my_audit_helper.php

Line Number: 176

Backtrace:

File: /var/www/html/application/helpers/my_audit_helper.php
Line: 176
Function: file_get_contents

File: /var/www/html/application/helpers/my_audit_helper.php
Line: 250
Function: simplexml_load_file_from_url

File: /var/www/html/application/helpers/my_audit_helper.php
Line: 3122
Function: getPubMedXML

File: /var/www/html/application/controllers/Detail.php
Line: 575
Function: pubMedSearch_Global

File: /var/www/html/application/controllers/Detail.php
Line: 489
Function: pubMedGetRelatedKeyword

File: /var/www/html/index.php
Line: 316
Function: require_once

N-(2-Chloro-eth-yl)morpholine-4-carbox-amide. | LitMetric

N-(2-Chloro-eth-yl)morpholine-4-carbox-amide.

Acta Crystallogr Sect E Struct Rep Online

Department of Pure and Industrial Chemistry, University of Nigeria, Nsukka, Enugu State, Nigeria.

Published: April 2014

The title compound, C7H13ClN2O2, synthesized by the reaction of 2-chloro-ethyl iso-cyanate and morpholine, crystallizes with four molecules in the asymmetric unit, which have similar conformations and comprise two pairs each related by approximate non-crystallographic inversion centres. Two of them have a modest orientational disorder of the 2-chloro-ethyl fragments [occupancy ratio of 0.778 (4):0.222 (4)]. In the crystal, mol-ecules are linked by N-H⋯O=C hydrogen bonds, forming three crystallographically different kinds of infinite hydrogen-bonded chains extending along [001].

Download full-text PDF

Source
http://www.ncbi.nlm.nih.gov/pmc/articles/PMC3998621PMC
http://dx.doi.org/10.1107/S1600536814005832DOI Listing

Publication Analysis

Top Keywords

n-2-chloro-eth-ylmorpholine-4-carbox-amide title
4
title compound
4
compound c7h13cln2o2
4
c7h13cln2o2 synthesized
4
synthesized reaction
4
reaction 2-chloro-ethyl
4
2-chloro-ethyl iso-cyanate
4
iso-cyanate morpholine
4
morpholine crystallizes
4
crystallizes molecules
4

Similar Publications

Want AI Summaries of new PubMed Abstracts delivered to your In-box?

Enter search terms and have AI summaries delivered each week - change queries or unsubscribe any time!