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Influence of heat curing on structure and physicochemical properties of phenolic acid loaded proteinaceous electrospun fibers. | LitMetric

AI Article Synopsis

  • * Heat curing at 150 °C for 24 hours altered the properties of the fiber mats based on the amount of gallic acid used, including a slower release rate of gallic acid.
  • * This research suggests that heat-cured zein-based fibers may be useful for food packaging applications due to their improved molecular structure and properties after treatment.

Article Abstract

Effects of heat treatment on structure and physicochemical properties of zein (Ze) and gallic acid loaded zein (Ze-GA) electrospun fiber mats were investigated. The electrospun fiber mats displayed different surface and physicochemical properties after being heat-cured at 150 °C for 24 h, which were closely related to the initial amount of loaded gallic acid. The gallic acid was released from the Ze-GA fiber mats in a constant manner, but heat curing decreased the rate of release. Heat curing remarkably increased the molecular weight of the Ze and Ze-GA electrospun fiber mats. Attenuated total reflectance Fourier transform infrared spectroscopy (ATR-FTIR) analysis of the fiber mats indicated variations in zein protein secondary structure after heat curing. (13)C solid state NMR (SS-NMR) confirmed the presence of a different chemical environment among the fiber mats. The fabrication of heat-cured zein based electrospun fibers in this study may find applications in the food packaging industry.

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Source
http://dx.doi.org/10.1021/jf500841mDOI Listing

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