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Direct condensation of functionalized sp(3) carbons with formanilides for enamine synthesis using an in situ generated HMDS amide catalyst. | LitMetric
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Direct condensation of functionalized sp(3) carbons with formanilides for enamine synthesis using an in situ generated HMDS amide catalyst.

Hiroshi Taneda Kiyofumi Inamoto Yoshinori Kondo

Chem Commun (Camb)

Graduate School of Pharmaceutical Sciences, Tohoku University, 6-3 Aoba, Aramaki, Aoba-ku, Sendai 980-8578, Japan.

Published: June 2014

The efficient synthesis of functionalized enamines including β-enaminoesters was effectively accomplished by the direct condensation of functionalized sp(3) carbanions such as acetates with formamides using in situ generated HMDS base from catalytic cesium fluoride and stoichiometric tristrimethylsilylamine.

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 Source
http://dx.doi.org/10.1039/c4cc02228aDOI Listing

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