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Direct dehydrative esterification of alcohols and carboxylic acids with a macroporous polymeric acid catalyst. | LitMetric
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Direct dehydrative esterification of alcohols and carboxylic acids with a macroporous polymeric acid catalyst.

Maki Minakawa Heeyoel Baek Yoichi M A Yamada Jin Wook Han Yasuhiro Uozumi

Org Lett

RIKEN Center for Sustainable Resource Science , Wako, Saitama 351-0198, Japan , Institute for Molecular Science , Okazaki, Aichi 444-8787, Japan , and Department of Chemistry, Hanyang University, Seoul 133-991, Korea.

Published: November 2013

A macroporous polymeric acid catalyst was prepared for the direct esterification of carboxylic acids and alcohols that proceeded at 50-80 °C without removal of water to give the corresponding esters with high yield. Flow esterification for the synthesis of biodiesel fuel was also achieved by using a column-packed macroporous acid catalyst under mild conditions without removal of water.

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http://dx.doi.org/10.1021/ol4028495DOI Listing

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