The objective of this study was to evaluate the effect of the concentration of calcium chloride (CaCl2) solution on the surface hardness of restorative glass ionomer cements (GICs). Two high-viscosity GICs, Fuji IX GP and GlasIonomer FX-II, were immersed in several concentrations of CaCl2 solution for 1 day and 1 week. The immersed specimen surfaces were evaluated using microhardness testing, grazing incidence X-ray diffraction, and energy-dispersive X-ray spectroscopy. Immersion in a higher concentration of CaCl2 solution produced a greater increase in the surface hardness. No crystalline substance was observed on the immersed surface. Calcium ions were selectively absorbed in the matrix of the GIC surface after immersion. They reacted with the non-reacted carboxylic acid groups remaining in the cement matrix. These reactions were considered to cause an increase in the surface hardness of the GICs.
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http://dx.doi.org/10.4012/dmj.2013-143 | DOI Listing |
Sci Rep
January 2025
Department of Prosthodontics, Yonsei University College of Dentistry, Yonsei-ro 50-1, Seodaemun-gu, Seoul, 03722, Republic of Korea.
The effects of heat-assisted vat photopolymerization (HVPP) on the physical and mechanical properties of 3D-printed dental resins, including the morphometric stability of 3D-printed crowns, were investigated. A resin tank was designed to maintain the resin at 30, 40, and 50 ℃ during the 3D printing process. Test specimens were fabricated using a commercial dental resin, with untreated resin serving as the control group.
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January 2025
Faculty of Engineering, Kitami Institute of Technology, 165 Koen-cho, Kitami 090-8507, Hokkaido, Japan.
The addition of hydrogen to nitrogen facilitates the formation of nitride phases in the plasma nitriding processes of stainless steels, though it also induces the deterioration of their mechanical properties. This study presents a hydrogen-free plasma nitriding process for fabricating a nitrogen-expanded austenite phase (γ) on an AISI 316 stainless steel surface. The steel substrate was nitrided in N-Ar plasma with various gas compositions discharged by radio frequency (RF) and direct current (DC) modes.
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December 2024
Department of Prosthodontics, Propaedeutics and Dental Materials, School of Dentistry, Christian-Albrechts University at Kiel, Arnold-Heller-Straße 16, 24105 Kiel, Germany.
This study was conducted to evaluate the material properties of polymer-infiltrated zinc oxide networks (PICN) and the effect of using a phosphate monomer-containing primer applied before polymer infiltration. A total of 148 ZnO-network (zinc oxide) specimens were produced: = 74 were treated with a primer before polymer infiltration and light curing, while the remaining specimens were untreated. Each group was divided into two subgroups ( = 37) based on the infiltrating polymer: UDMA (aliphatic urethane-dimethacrylates)-TEGDMA (triethylene glycol-dimethacrylate) or BisGMA (bisphenol A-glycidyl-methacrylate)-TEGDMA.
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December 2024
School of Material Science and Engineering, Shandong Jianzhu University, Jinan 250101, China.
Wire-arc additive manufacturing (WAAM) has fully empowered the design and manufacturing of metals with its unparalleled efficiency and flexibility. However, the process has relatively poor shape control capabilities, often requiring machining post-processing. This study explores a tungsten inert gas arc remelting (TIGAR) process to improve the surface flatness of WAAM components at a low cost and significantly reduce machining waste (up to 76%), which is crucial for the sustainable development of the process.
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December 2024
School of Materials Science and Engineering, Henan University of Science and Technology, Luoyang 471023, China.
Copper matrix composites (Cu-MCs) have garnered significant attention due to their exceptional electrical, wear-resistant, and mechanical properties. Among them, AlO/Cu composites, reinforced with AlO, are a focal point in the field of high-strength, high-conductivity copper alloys, owing to their high strength, excellent electrical conductivity, and superior resistance to high-temperature softening. Cold deformation is an effective method for enhancing the mechanical properties of AlO/Cu composites.
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